1-[(dimethyl-lambda~4~-sulfanylidene)amino]-4-nitrobenzene

Base Information

Chemical Name:1-[(dimethyl-lambda~4~-sulfanylidene)amino]-4-nitrobenzene
CAS No.:27691-52-7
Molecular Formula:C₈H₁₀N₂O₂S
Molecular Weight:198.246
Hs Code.:
Mol file:27691-52-7.mol

Synonyms:Sulfilimine,S,S-dimethyl-N-(4-nitrophenyl)- (9CI); Sulfilimine,S,S-dimethyl-N-(p-nitrophenyl)- (8CI); N-4-Nitrophenyl-S,S-dimethylsulfimide;NSC 287993

Suppliers and Price of 1-[(dimethyl-lambda~4~-sulfanylidene)amino]-4-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-[(dimethyl-lambda~4~-sulfanylidene)amino]-4-nitrobenzene

Chemical Property:

Vapor Pressure:2.1E-05mmHg at 25°C
Boiling Point:372.2°C at 760 mmHg
Flash Point:178.9°C
Density:1.29g/cm³

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-[(dimethyl-lambda~4~-sulfanylidene)amino]-4-nitrobenzene

There total 4 articles about 1-[(dimethyl-lambda~4~-sulfanylidene)amino]-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 100-01-6,104810-17-5
4-nitro-aniline

: 27691-52-7,880487-08-1
S,S-dimethyl-N-(p-nitrophenyl)sulfilimine

Guidance literature:: Multistep reaction; (i) P₂O₅, DMF, (ii) /BRN= 508690/, (iii) Et₃N;
DOI:10.1016/0040-4020(78)87005-7

Reference yield:

: 1516-60-5
4-nitrophenyl azide

: 27691-52-7,880487-08-1
S,S-dimethyl-N-(p-nitrophenyl)sulfilimine

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent Chromat_. / trifluoroacetic acid (TFA), trifluoromethanesulphonic acid (TFSA) / 4 h / 25 °C

2: 1.) trifluoroacetic anhydride (TFAA) / 1.) CH₂Cl₂, -60 deg C, 2.) a) -60 deg C, 2 h, b) from -60 deg C to RT

With trifluorormethanesulfonic acid; trifluoroacetic acid; trifluoroacetic anhydride;