Hexanoic acid, 2-butyl-2-hydroxy-, 2-(4-bromophenyl)hydrazide

Base Information

• Chemical Name: Hexanoic acid, 2-butyl-2-hydroxy-, 2-(4-bromophenyl)hydrazide
• CAS No.: 7368-88-9
• Molecular Formula: C16H25BrN2O2
• Molecular Weight: 357.28600

Synonyms:Dibutylglykolsaeure-4-brom-phenylhydrazid;2-Butyl-2-hydroxy-hexanoic acid N'-(4-bromo-phenyl)-hydrazide;Di-n-butylglykolsaeure-M2-4-bromphenylhydrazid;2-Butyl-2-hydroxy-hexansaeure-[N'-(4-brom-phenyl)-hydrazid];2-butyl-2-hydroxy-hexanoic acid-[N'-(4-bromo-phenyl)-hydrazide];

Chemical Property of Hexanoic acid, 2-butyl-2-hydroxy-, 2-(4-bromophenyl)hydrazide

Chemical Property:

• Melting Point: 135 - 136 °C (toluene)
• PSA: 61.36000
• LogP: 4.46760

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Hexanoic acid, 2-butyl-2-hydroxy-, 2-(4-bromophenyl)hydrazide

There total 1 articles about Hexanoic acid, 2-butyl-2-hydroxy-, 2-(4-bromophenyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

n-butyl magnesium bromide (693-03-8) + oxalic acid ethyl ester-[N'-(4-bromo-phenyl)-hydrazide] (39771-61-4) → dibutylglycolic acid p-bromophenylhydrazide (7368-88-9)

Guidance literature:

Reference yield: 73.0%

4-bromo-phenol (106-41-2) + dibutylglycolic acid p-bromophenylhydrazide (7368-88-9) → α-chloro-α-butylcaproic acid p-bromophenylhydrazide*p-bromophenol

Guidance literature:

With phosphorus pentachloride; In 1,4-dioxane; at 5 - 25 ℃; for 30h;

Reference yield: 64.0%

dibutylglycolic acid p-bromophenylhydrazide (7368-88-9) + phenol (108-95-2,27073-41-2) → 2-Butyl-2-chloro-hexanoic acid N'-(4-bromo-phenyl)-hydrazide; compound with phenol (95101-29-4)

Guidance literature:

With phosphorus pentachloride; In 1,4-dioxane; 1.) 12 h, 20 deg C; 2.) 24 h, then 2 days in the refrigerator;

upstream raw materials:

n-butyl magnesium bromide

oxalic acid ethyl ester-[N'-(4-bromo-phenyl)-hydrazide]

Downstream raw materials:

2-Butyl-2-chloro-hexanoic acid N'-(4-bromo-phenyl)-hydrazide; compound with phenol

2--4-(p-bromophenyl)-6,6-diphenyl-4,5-dihydro-6H-1,3,4-oxadiazinone-5

2-Butyl-2-chloro-hexanoic acid N'-(4-bromo-phenyl)-hydrazide

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