Technology Process of 2(5H)-Furanone, 4-methoxy-5-(1-methoxy-3-phenyl-2-propenylidene)-,
(E,E)-
There total 8 articles about 2(5H)-Furanone, 4-methoxy-5-(1-methoxy-3-phenyl-2-propenylidene)-,
(E,E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85 percent / H2 / Lindlar cat. / tetrahydrofuran; hexane / 0.42 h / Ambient temperature
2: 83 percent / amberlyst, methyl orthoformate / methanol / 48 h / Ambient temperature
3: Lithium methoxide / benzene; toluene / 240 h / Heating
With
Amberlyst; lithium methanolate; hydrogen; trimethyl orthoformate;
Lindlar catalyst;
In
tetrahydrofuran; methanol; hexane; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) BF3*Et2O / 1.)diethyl ether, -78 deg C, 2 h, 2.) -78 deg C, 1 h, RT., 16 h
2: 85 percent / H2 / Lindlar cat. / tetrahydrofuran; hexane / 0.42 h / Ambient temperature
3: 83 percent / amberlyst, methyl orthoformate / methanol / 48 h / Ambient temperature
4: Lithium methoxide / benzene; toluene / 240 h / Heating
With
Amberlyst; boron trifluoride diethyl etherate; lithium methanolate; hydrogen; trimethyl orthoformate;
Lindlar catalyst;
In
tetrahydrofuran; methanol; hexane; toluene; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 83 percent / amberlyst, methyl orthoformate / methanol / 48 h / Ambient temperature
2: Lithium methoxide / benzene; toluene / 240 h / Heating
With
Amberlyst; lithium methanolate; trimethyl orthoformate;
In
methanol; toluene; benzene;
