2-(Benzenesulfonyl)-1-cyclopropylethan-1-one

Base Information

Chemical Name:2-(Benzenesulfonyl)-1-cyclopropylethan-1-one
CAS No.:74480-95-8
Molecular Formula:C11H12O3S
Molecular Weight:224.28
Hs Code.:
DSSTox Substance ID:DTXSID60502838
Wikidata:Q82356194

Synonyms:74480-95-8;2-(Benzenesulfonyl)-1-cyclopropylethan-1-one;DTXSID60502838;AKOS013223068

Suppliers and Price of 2-(Benzenesulfonyl)-1-cyclopropylethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(Benzenesulfonyl)-1-cyclopropylethan-1-one

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:224.05071541
Heavy Atom Count:15
Complexity:329

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC1C(=O)CS(=O)(=O)C2=CC=CC=C2

Technology Process of 2-(Benzenesulfonyl)-1-cyclopropylethan-1-one

There total 5 articles about 2-(Benzenesulfonyl)-1-cyclopropylethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 69267-75-0
2-bromo-1-cyclopropylethan-1-one

: 618-41-7
Benzenesulfinic acid

: 74480-95-8
1-cyclopropyl-2-(phenylsulfonyl)ethan-1-one

Guidance literature:: In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.202004658

Reference yield: 80.0%

: 3959-23-7
benzenesulfonylacetic acid

: 4023-34-1
cyclopropanecarboxylic acid chloride

: 74480-95-8
1-cyclopropyl-2-(phenylsulfonyl)ethan-1-one

Guidance literature:: benzenesulfonylacetic acid; With [2,2]bipyridinyl; n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere;

cyclopropanecarboxylic acid chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/bkcs.10591

Reference yield: 65.0%

: 63772-71-4
3-cyclopropyl-3-oxopropanoic acid

: 873-55-2
sodium benzenesulfonate

: 74480-95-8
1-cyclopropyl-2-(phenylsulfonyl)ethan-1-one

Guidance literature:: With potassium phosphate; N-Bromosuccinimide; In dichloromethane; at 20 ℃; for 24h; chemoselective reaction; Schlenk technique;
DOI:10.1016/j.tet.2018.08.024