Cyclohexanone, 3,3,5,5-tetramethyl-2-nitro-

Base Information

Chemical Name:Cyclohexanone, 3,3,5,5-tetramethyl-2-nitro-
CAS No.:74609-83-9
Molecular Formula:C10H17NO3
Molecular Weight:199.25
Hs Code.:
DSSTox Substance ID:DTXSID30452134
Nikkaji Number:J765.025F

Synonyms:74609-83-9;Cyclohexanone, 3,3,5,5-tetramethyl-2-nitro-;DTXSID30452134;2-Nitro-3,3,5,5-tetramethylcyclohexanone

Suppliers and Price of Cyclohexanone, 3,3,5,5-tetramethyl-2-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanone, 3,3,5,5-tetramethyl-2-nitro-

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:199.12084340
Heavy Atom Count:14
Complexity:276

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CC(=O)C(C(C1)(C)C)[N+](=O)[O-])C

Technology Process of Cyclohexanone, 3,3,5,5-tetramethyl-2-nitro-

There total 2 articles about Cyclohexanone, 3,3,5,5-tetramethyl-2-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 56763-68-9
Enol acetate of 3,3,5,5-tetramethylcyclohexanone

: 74609-83-9
2-nitro-3,3,5,5-tetramethylcyclohexanone

Guidance literature:: With ammonium nitrate; trifluoroacetic anhydride; In chloroform; for 1h; Ambient temperature;
DOI:10.1055/s-1983-30417

Reference yield:

: 14376-79-5
3,3,5,5-tetramethylcyclohexanone

: 74609-83-9
2-nitro-3,3,5,5-tetramethylcyclohexanone

Guidance literature:: With n-Amyl nitrite; potassium hydride; Yield given. Multistep reaction; 1) DME, rt, 2) DME, -78 deg C to rt;
DOI:10.1021/jo00338a017