2-Cyclohexen-1-one, 2-methyl-4-(1-methylethenyl)-

Base Information

Chemical Name:2-Cyclohexen-1-one, 2-methyl-4-(1-methylethenyl)-
CAS No.:74852-25-8
Molecular Formula:C10H14O
Molecular Weight:150.221
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyclohexen-1-one, 2-methyl-4-(1-methylethenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Cyclohexen-1-one, 2-methyl-4-(1-methylethenyl)-

There total 6 articles about 2-Cyclohexen-1-one, 2-methyl-4-(1-methylethenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74852-23-6,135942-83-5
(2S,5S)-5-Isopropenyl-2-methyl-2-phenylsulfanyl-cyclohexanone

: 99-49-0,22327-39-5
Carvone

: 74852-25-8
(+/-)-sylvecarvone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; phosphorous acid trimethyl ester; Yield given. Multistep reaction; 1.) methylene chloride, -78 deg C, 30 min, room temperature, 1 h, 2.) reflux, 8 h;
DOI:10.1021/ja00530a041

Reference yield:

: 60603-24-9
5-Isopropenyl-2-phenylsulfanyl-cyclohexanone

: 74852-25-8
(+/-)-sylvecarvone

Guidance literature:: Multi-step reaction with 2 steps

1: 158 mg / sodium hydride / tetrahydrofuran / 4 h / 20 °C

2: 1.) MCPBA, 2.) trimethyl phosphite / 1.) methylene chloride, -78 deg C, 30 min, room temperature, 1 h, 2.) reflux, 8 h

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; phosphorous acid trimethyl ester; In tetrahydrofuran;
DOI:10.1021/ja00530a041

Reference yield:

: 74852-19-0
(4-Isopropenyl-2-methoxy-cyclohex-1-enylsulfanyl)-benzene

: 74852-25-8
(+/-)-sylvecarvone

Guidance literature:: Multi-step reaction with 3 steps

1: 130 mg / aq. perchloric acid / acetonitrile / 4 h / 0 °C

2: 158 mg / sodium hydride / tetrahydrofuran / 4 h / 20 °C

3: 1.) MCPBA, 2.) trimethyl phosphite / 1.) methylene chloride, -78 deg C, 30 min, room temperature, 1 h, 2.) reflux, 8 h

With perchloric acid; sodium hydride; 3-chloro-benzenecarboperoxoic acid; phosphorous acid trimethyl ester; In tetrahydrofuran; acetonitrile;
DOI:10.1021/ja00530a041