Rhodium(1+), carbonyl(2-propanone)bis(triphenylphosphine)-,perchlorate

Base Information

Chemical Name:Rhodium(1+), carbonyl(2-propanone)bis(triphenylphosphine)-,perchlorate
CAS No.:75214-93-6
Molecular Formula:C₄₀H₃₆O₂P₂Rh*ClO₄
Molecular Weight:813.028
Hs Code.:

Synonyms:Rhodium(1+), carbonyl(2-propanone)bis(triphenylphosphine)-,perchlorate

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Chemical Property of Rhodium(1+), carbonyl(2-propanone)bis(triphenylphosphine)-,perchlorate

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Technology Process of Rhodium(1+), carbonyl(2-propanone)bis(triphenylphosphine)-,perchlorate

There total 1 articles about Rhodium(1+), carbonyl(2-propanone)bis(triphenylphosphine)-,perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 15318-33-9,16353-77-8,13938-94-8
chlorocarbonylbis(triphenylphosphine)rhodium(I)

: silver perchlorate

: 75214-93-6,32334-51-3
[CO(P(C₆H₅)3)2RhCH₃COCH₃]⁽¹⁺⁾*ClO₄^(1-) = [CO(P(C₆H₅)3)2RhCH₃COCH₃]ClO₄

Guidance literature:: With acetone; In acetone; byproducts: AgCl; silver compd. soln. added to Rh-compd. suspn. in acetone, stirred for 5min; ppt. filtered, solvent evapd. to a small volume, diethyl ether added, product crystd.; elem.anal.;
DOI:10.1039/DT9800001259

Reference yield: 87.0%

: 230-27-3
7,8-benzoquinoline

: 75214-93-6,32334-51-3
[CO(P(C₆H₅)3)2RhCH₃COCH₃]⁽¹⁺⁾*ClO₄^(1-) = [CO(P(C₆H₅)3)2RhCH₃COCH₃]ClO₄

: [Rh(CO)(PPh₃)2(bquin)][ClO₄]*2CHCl₃ bquin

Guidance literature:: With chloroform; In chloroform; org. compd. added to metal compd. soln. in 1.4/1 mol ratio; product crystd.; elem.anal.;
DOI:10.1039/DT9800001259

Reference yield: 81.0%

: 75214-93-6,32334-51-3
[CO(P(C₆H₅)3)2RhCH₃COCH₃]⁽¹⁺⁾*ClO₄^(1-) = [CO(P(C₆H₅)3)2RhCH₃COCH₃]ClO₄

: 108792-66-1
[Rh(C₆H₄C₆H₂F₄)(C₅H₄NNC₅H₄N)]

: 108792-77-4
[(C₆H₄C₆H₂F₄)Rh(C₅H₄NNC₅H₄N)Rh(CO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[(C₆H₄C₆H₂F₄)Rh(C₅H₄NNC₅H₄N)Rh(CO)(P(C₆H₅)3)2]ClO₄

Guidance literature:: In dichloromethane; addn. of solid phosphine complex to diolefin complex soln., room temp.; evapn. to small volume, addn. of Et2O, crystn., filtration; elem. anal.;
DOI:10.1016/S0020-1693(00)87699-9