3-Quinolinemethanol, 2-amino-

Base Information

• Chemical Name: 3-Quinolinemethanol, 2-amino-
• CAS No.: 75353-55-8
• Molecular Formula: C₁₀H₁₀N₂O
• Molecular Weight: 174.202

Synonyms:2-amino-3-formylquinoline;2-amino-3-(hydroxymethyl)quinoline;amino-2 aza-1-azulene;2-Amino-1-azaazulene;2-aminoquinoline-3-carbaldehyde;2-aminocycloheptapyrrole;amino-2 hydroxymethyl-3 quinoleine;amino-2 formyl-3 quinoleine;

Chemical Property of 3-Quinolinemethanol, 2-amino-

Chemical Property:

• PSA: 59.87000
• LogP: 1.23940

Purity/Quality:

99% ^*data from raw suppliers

2-amino-3-Quinolinemethanol 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Quinolinemethanol, 2-amino-

There total 3 articles about 3-Quinolinemethanol, 2-amino- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

methyl 2-aminoquinoline-3-carboxylate (75353-50-3) → amino-2 hydroxymethyl-3 quinoleine (75353-55-8)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Heating;

Reference yield: 68.0%

ethyl 2-aminoquinoline-3-carboxylate (36926-83-7) → amino-2 hydroxymethyl-3 quinoleine (75353-55-8)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Heating;

DOI:10.1021/jm00401a009

Reference yield:

acide amino-2 quinoleine carboxylique-3 (31407-29-1) → amino-2 hydroxymethyl-3 quinoleine (75353-55-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / H₂SO₄ (conc.) / 7 h / Heating

2: 87 percent / lithium aluminium hydride / tetrahydrofuran / 1 h / Heating

With lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran;

upstream raw materials:

methyl 2-aminoquinoline-3-carboxylate

ethyl 2-aminoquinoline-3-carboxylate

acide amino-2 quinoleine carboxylique-3

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