1H-Pyrrole-2-carboxylic acid, 4-(2-chloroethyl)-5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1 H-pyrrol-2-yl]methyl]-3-methyl-, phenylmethyl ester

Base Information

Chemical Name:1H-Pyrrole-2-carboxylic acid, 4-(2-chloroethyl)-5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1 H-pyrrol-2-yl]methyl]-3-methyl-, phenylmethyl ester
CAS No.:75488-04-9
Molecular Formula:C28H35ClN2O4
Molecular Weight:499.05
Hs Code.:

1H-Pyrrole-2-carboxylic acid,
4-(2-chloroethyl)-5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1
H-pyrrol-2-yl]methyl]-3-methyl-, phenylmethyl ester

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Chemical Property of 1H-Pyrrole-2-carboxylic acid, 4-(2-chloroethyl)-5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1 H-pyrrol-2-yl]methyl]-3-methyl-, phenylmethyl ester

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Technology Process of 1H-Pyrrole-2-carboxylic acid, 4-(2-chloroethyl)-5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1 H-pyrrol-2-yl]methyl]-3-methyl-, phenylmethyl ester

There total 1 articles about 1H-Pyrrole-2-carboxylic acid, 4-(2-chloroethyl)-5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1 H-pyrrol-2-yl]methyl]-3-methyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 75488-16-3
tert-Butyl-(3-ethyl-4-methyl-pyrrolyl-2)-methanoat

: 37945-74-7
benzyl 5-acetoxymethyl-4-(2-chloroethyl)-3-methylpyrrole-2-carboxylate

: 75488-04-9
benzyl 5'-(t-butyloxycarbonyl)-3-(2-chloroethyl)-4'-ethyl-3',4-dimethyldipyrrylmethane-5-carboxylate

Guidance literature:: With toluene-4-sulfonic acid; In acetic acid; at 40 ℃; for 5h;

Reference yield: 70.0%

: 2199-59-9
ethyl (5-formyl-2,4-dimethyl-1H-pyrrole)-3-carboxylate

: 75488-04-9
benzyl 5'-(t-butyloxycarbonyl)-3-(2-chloroethyl)-4'-ethyl-3',4-dimethyldipyrrylmethane-5-carboxylate

: 112452-50-3
benzyl 2-(2-chloroethyl)-6-ethoxycarbonyl-4-ethyl-1,3,5,6'-tetramethyltripyrrene-1'-carboxylic acid hydrobromide

Guidance literature:: With trifluoroacetic acid; In methanol; for 0.0833333h; Ambient temperature;

Reference yield:

: 75488-04-9
benzyl 5'-(t-butyloxycarbonyl)-3-(2-chloroethyl)-4'-ethyl-3',4-dimethyldipyrrylmethane-5-carboxylate

: 112452-55-8
4-(2-chloroethyl)-8-ethoxycarbonyl-6-ethyl-1',1-bis(2-methoxycarbonylethyl)-2,3,5,7,8'-pentamethyl-a,c-biladiene dihydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / trifluoroacetic acid / methanol / 0.08 h / Ambient temperature

2: 81 percent / trifluoroacetic acid, HBr (31percent) / methanol; acetic acid / 0.5 h

With hydrogen bromide; trifluoroacetic acid; In methanol; acetic acid;