3,5-Dimethoxybenzoyl azide

Base Information

Chemical Name:3,5-Dimethoxybenzoyl azide
CAS No.:75996-26-8
Molecular Formula:C9H9N3O3
Molecular Weight:207.189
Hs Code.:
DSSTox Substance ID:DTXSID20505941
Wikidata:Q82361407

Synonyms:3,5-Dimethoxybenzoyl azide;75996-26-8;DTXSID20505941;AKOS006034677

Suppliers and Price of 3,5-Dimethoxybenzoyl azide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Dimethoxybenzoyl azide

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:207.06439116
Heavy Atom Count:15
Complexity:264

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1)C(=O)N=[N+]=[N-])OC

Technology Process of 3,5-Dimethoxybenzoyl azide

There total 6 articles about 3,5-Dimethoxybenzoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 17213-57-9
3,5-dimethoxybenzoyl chloride

: 75996-26-8
azido(3,5-dimethoxyphenyl)methanone

Guidance literature:: With sodium azide; In water; acetone; for 1h; Cooling;
DOI:10.1039/c8dt03225d

Reference yield: 77.0%

: 1132-21-4
3,5-dimethoxybenzoic acid

: 75996-26-8
azido(3,5-dimethoxyphenyl)methanone

Guidance literature:: 3,5-dimethoxybenzoic acid; With oxalyl dichloride; In acetone; toluene; Heating;

With sodium azide; In water; acetone; for 12h; Further stages.;
DOI:10.1021/jo991661l