1H-Indazole-3-carboxylic acid, 1-phenyl-

Base Information

Chemical Name:1H-Indazole-3-carboxylic acid, 1-phenyl-
CAS No.:7716-36-1
Molecular Formula:C14H10N2O2
Molecular Weight:238.246
Hs Code.:

Synonyms:

Suppliers and Price of 1H-Indazole-3-carboxylic acid, 1-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 5 raw suppliers

Chemical Property of 1H-Indazole-3-carboxylic acid, 1-phenyl-

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Indazole-3-carboxylic acid, 1-phenyl-

There total 6 articles about 1H-Indazole-3-carboxylic acid, 1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: methyl 2-(2-chlorophenyl)-2-(2-phenylhydrazono)acetate

: 7716-36-1
1-phenyl-1H-indazole-3-carboxylic acid

Guidance literature:: methyl 2-(2-chlorophenyl)-2-(2-phenylhydrazono)acetate; With copper(l) iodide; caesium carbonate; L-proline; In dimethyl sulfoxide; at 75 - 80 ℃; for 6h;

With hydrogenchloride; In water; toluene; pH=2 - 2.5;
DOI:10.1002/jhet.1717

Reference yield:

: 2-(2-chlorophenyl)-2-oxoacetamide

: 7716-36-1
1-phenyl-1H-indazole-3-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 4.5 h / 40 - 64 °C

2.1: potassium carbonate / isopropyl alcohol / 6 h / 60 - 65 °C

3.1: L-proline; caesium carbonate; copper(l) iodide / dimethyl sulfoxide / 6 h / 75 - 80 °C

3.2: pH 2 - 2.5

With copper(l) iodide; thionyl chloride; potassium carbonate; caesium carbonate; L-proline; In dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1002/jhet.1717

Reference yield:

: 34966-49-9
methyl 2-chlorobenzoylformate

: 7716-36-1
1-phenyl-1H-indazole-3-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / isopropyl alcohol / 6 h / 60 - 65 °C

2.1: L-proline; caesium carbonate; copper(l) iodide / dimethyl sulfoxide / 6 h / 75 - 80 °C

2.2: pH 2 - 2.5

With copper(l) iodide; potassium carbonate; caesium carbonate; L-proline; In dimethyl sulfoxide; isopropyl alcohol;
DOI:10.1002/jhet.1717