5-Nitronaphthalene-2,3-diol

Base Information

Chemical Name:5-Nitronaphthalene-2,3-diol
CAS No.:77542-54-2
Molecular Formula:C10H7NO4
Molecular Weight:205.17
Hs Code.:2908999090
DSSTox Substance ID:DTXSID10453442
Wikidata:Q72495026
Mol file:77542-54-2.mol

Synonyms:5-nitronaphthalene-2,3-diol;77542-54-2;5-nitro-2,3-dihydroxynaphthalene;SCHEMBL419966;DTXSID10453442;LDYYFPIQYNIWIW-UHFFFAOYSA-N;MFCD21340267;BS-50492;CS-0199471;FT-0747624

Suppliers and Price of 5-Nitronaphthalene-2,3-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
5-Nitronaphthalene-2,3-diol 97%
1g
$ 614.00

Chemenu
5-nitronaphthalene-2,3-diol 97%
1g
$ 580.00

American Custom Chemicals Corporation
5-NITRONAPHTHALENE-2,3-DIOL 95.00%
5MG
$ 504.05

Alichem
5-Nitronaphthalene-2,3-diol
1g
$ 992.16

Total 8 raw suppliers

Chemical Property of 5-Nitronaphthalene-2,3-diol

Chemical Property:

Melting Point:207-209℃
PSA：86.28000
LogP:2.68240
Storage Temp.:Inert atmosphere,Room Temperature
XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:205.03750770
Heavy Atom Count:15
Complexity:252

Purity/Quality:

99% ^*data from raw suppliers

5-Nitronaphthalene-2,3-diol 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=CC(=C(C=C2C(=C1)[N+](=O)[O-])O)O

Technology Process of 5-Nitronaphthalene-2,3-diol

There total 3 articles about 5-Nitronaphthalene-2,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 56517-24-9
6,7-bis(methylsulfonyloxy)-1-nitronaphthalene

: 77542-54-2
5-nitro-2,3-dihydroxynaphthalene

Guidance literature:: With sodium hydroxide; In water; at 100 ℃;
DOI:10.3987/COM-15-S(T)56

Reference yield:

: 92-44-4
2,3-naphthalenediol

: 77542-54-2
5-nitro-2,3-dihydroxynaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / chloroform / 0 °C

2: acetic anhydride; nitric acid / 37 - 39 °C

3: sodium hydroxide; water / 100 °C

With water; nitric acid; acetic anhydride; triethylamine; sodium hydroxide; In chloroform;
DOI:10.1016/j.bmcl.2012.09.097

Reference yield:

: 22426-45-5
2,3-bis(methylsulfonyloxy)naphthalene

: 77542-54-2
5-nitro-2,3-dihydroxynaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride; nitric acid / 37 - 39 °C

2: sodium hydroxide; water / 100 °C

With water; nitric acid; acetic anhydride; sodium hydroxide;
DOI:10.1016/j.bmcl.2012.09.097