Cycloundecanol, 4-methylbenzenesulfonate

Base Information

• Chemical Name: Cycloundecanol, 4-methylbenzenesulfonate
• CAS No.: 78052-04-7
• Molecular Formula: C₁₈H₂₈O₃S
• Molecular Weight: 324.485
• Mol file: 78052-04-7.mol

Synonyms:

Chemical Property of Cycloundecanol, 4-methylbenzenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cycloundecanol, 4-methylbenzenesulfonate

There total 2 articles about Cycloundecanol, 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cycloundecanone (878-13-7) → toluene-4-sulfonic acid cycloundecyl ester (78052-04-7)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium alanate; diethyl ether

With lithium aluminium tetrahydride; diethyl ether;

DOI:10.1021/ja01593a024

Reference yield:

cycloundecanol (24469-57-6) + p-toluenesulfonyl chloride (98-59-9) → toluene-4-sulfonic acid cycloundecyl ester (78052-04-7)

Guidance literature:

DOI:10.1021/ja01593a024 DOI:10.1002/hlca.19550380629

Reference yield:

toluene-4-sulfonic acid cycloundecyl ester (78052-04-7) → cycloundecanol (24469-57-6)

Guidance literature:

With 1,1,1,3',3',3'-hexafluoro-propanol; water; at 24.9 ℃; Rate constant; Thermodynamic data; ΔG, ΔH, ΔS;

DOI:10.1021/jo00369a010

upstream raw materials:

cycloundecanol

p-toluenesulfonyl chloride

cycloundecanone

Downstream raw materials:

cycloundecanol