4-Bromo-2,3,6-trichloroanisole

Base Information

Chemical Name:4-Bromo-2,3,6-trichloroanisole
CAS No.:78647-87-7
Molecular Formula:C7H4BrCl3O
Molecular Weight:290.371
Hs Code.:
DSSTox Substance ID:DTXSID601335050
Nikkaji Number:J1.617.541B

Synonyms:4-Bromo-2,3,6-trichloroanisole;1-bromo-2,3,5-trichloro-4-methoxybenzene;78647-87-7;VZRSUQWPXPUWCS-UHFFFAOYSA-N;DTXSID601335050

Suppliers and Price of 4-Bromo-2,3,6-trichloroanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Bromo-2,3,6-trichloroanisole

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:287.85111
Heavy Atom Count:12
Complexity:158

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1Cl)Br)Cl)Cl

Technology Process of 4-Bromo-2,3,6-trichloroanisole

There total 5 articles about 4-Bromo-2,3,6-trichloroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 13311-72-3
2,3,6-trichloro-4-bromophenol

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 78647-87-7
4-bromo-2,3,6-trichloroanisole

Guidance literature:: 2,3,6-trichloro-4-bromophenol; dimethyl sulfoxide; With sodium hydroxide;

for 0.5h; Heating;
DOI:10.1016/S0045-6535(01)00052-2

Reference yield:

: 933-75-5
2,3,6-trichlorophenol

: 78647-87-7
4-bromo-2,3,6-trichloroanisole

Guidance literature:: Multi-step reaction with 2 steps

1.1: 67 percent / Br / acetic acid

2.1: aque. NaOH

2.2: 27 percent / 0.5 h / Heating

With sodium hydroxide; bromine; In acetic acid;
DOI:10.1016/S0045-6535(01)00052-2

Reference yield:

: 64981-10-8
2,3,6-trichloro p-aminophenol

: 78647-87-7
4-bromo-2,3,6-trichloroanisole

Guidance literature:: Multi-step reaction with 3 steps

1: aqueous HCl / Diazotization_.Kochen der Diazoniumsalz-Loesung mit Aethanol

2: glacial acetic acid; bromine

3: aqueous KOH

With hydrogenchloride; potassium hydroxide; bromine; acetic acid;