2-Cyclohexen-1-one, 2,2'-dithiobis[3-hydroxy-5,5-dimethyl-

Base Information

Chemical Name:2-Cyclohexen-1-one, 2,2'-dithiobis[3-hydroxy-5,5-dimethyl-
CAS No.:78663-71-5
Molecular Formula:C₁₆H₂₂O₄S₂
Molecular Weight:342.48
Hs Code.:
DSSTox Substance ID:DTXSID20401999
Nikkaji Number:J2.514.410D
Wikidata:Q82205338

Synonyms:78663-71-5;2-Cyclohexen-1-one, 2,2'-dithiobis[3-hydroxy-5,5-dimethyl-;DTXSID20401999;2,2'-Dithiobis(3-hydroxy-5,5-dimethyl-2-cyclohexene-1-one)

Suppliers and Price of 2-Cyclohexen-1-one, 2,2'-dithiobis[3-hydroxy-5,5-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-Cyclohexen-1-one, 2,2'-dithiobis[3-hydroxy-5,5-dimethyl-

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:342.09595153
Heavy Atom Count:22
Complexity:533

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CC(=C(C(=O)C1)SSC2=C(CC(CC2=O)(C)C)O)O)C

Technology Process of 2-Cyclohexen-1-one, 2,2'-dithiobis[3-hydroxy-5,5-dimethyl-

There total 3 articles about 2-Cyclohexen-1-one, 2,2'-dithiobis[3-hydroxy-5,5-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 955402-05-8
5,5-dimethyl-2-sulfanylcyclohexan-1,3-dion

: 78663-71-5
2,2'-disulfanediylbis(3-hydroxy-5,5-dimethylcyclohex-2-en-1-on)

Guidance literature:: With sodium hydroxide; oxygen;
DOI:10.1002/hlca.200790169

Reference yield:

: 1195-91-1
2-bromodimedone

: 78663-71-5
2,2'-disulfanediylbis(3-hydroxy-5,5-dimethylcyclohex-2-en-1-on)

Guidance literature:: Multi-step reaction with 3 steps

1.1: 97 percent / AcONa / H₂O / 0 °C

2.1: aq. NaOH / 0.5 h / 40 - 50 °C

2.2: 83 percent / aq. HCl / pH 2 - 3

3.1: 92 percent / aq. NaOH; O₂

With sodium hydroxide; oxygen; sodium acetate; In water;
DOI:10.1002/hlca.200790169

Reference yield:

: 2-{[amino(iminio)methyl]sulfanyl}-5,5-dimethyl-3-oxocyclohex-1-en-1-olat

: 78663-71-5
2,2'-disulfanediylbis(3-hydroxy-5,5-dimethylcyclohex-2-en-1-on)

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. NaOH / 0.5 h / 40 - 50 °C

1.2: 83 percent / aq. HCl / pH 2 - 3

2.1: 92 percent / aq. NaOH; O₂

With sodium hydroxide; oxygen;
DOI:10.1002/hlca.200790169