tert-Butyl (4-nitrobenzoyl)oxycarbamate

Base Information

Chemical Name:tert-Butyl (4-nitrobenzoyl)oxycarbamate
CAS No.:35657-41-1
Molecular Formula:C12H14N2O6
Molecular Weight:282.253
Hs Code.:
NSC Number:191037
DSSTox Substance ID:DTXSID10307436
Nikkaji Number:J3.195.909H
Wikidata:Q82054839
Mol file:35657-41-1.mol

Synonyms:tert-Butyl (4-nitrobenzoyl)oxycarbamate;35657-41-1;[(2-methylpropan-2-yl)oxycarbonylamino] 4-nitrobenzoate;NSC191037;tert-butyl ((4-nitrobenzoyl)oxy)carbamate;SCHEMBL15058771;DTXSID10307436;AMY23894;MFCD28101705;AKOS024262243;tert-Butyl(4-nitrobenzoyl)oxycarbamate;DS-3193;NSC-191037;[(tert-butoxy)carbonyl]amino 4-nitrobenzoate;CS-0154354;I10079;A874552

Suppliers and Price of tert-Butyl (4-nitrobenzoyl)oxycarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
tert-Butyl(4-nitrobenzoyl)oxycarbamate >95%
1g
$ 630.00

Crysdot
tert-Butyl(4-nitrobenzoyl)oxycarbamate 95+%
1g
$ 313.00

Ambeed
tert-Butyl(4-nitrobenzoyl)oxycarbamate 95%
5g
$ 138.00

Ambeed
tert-Butyl(4-nitrobenzoyl)oxycarbamate 95%
1g
$ 44.00

Ambeed
tert-Butyl(4-nitrobenzoyl)oxycarbamate 95%
250mg
$ 17.00

Ambeed
tert-Butyl(4-nitrobenzoyl)oxycarbamate 95%
100mg
$ 11.00

Abosyn
tert-Butyl(4-nitrobenzoyl)oxycarbamate 95-98%
1g
$ 315.00

Total 14 raw suppliers

Chemical Property of tert-Butyl (4-nitrobenzoyl)oxycarbamate

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：110.45000
Density:1.297g/cm³
LogP:3.10540
Storage Temp.:Sealed in dry,Room Temperature
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:282.08518617
Heavy Atom Count:20
Complexity:376

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl(4-nitrobenzoyl)oxycarbamate >95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NOC(=O)C1=CC=C(C=C1)[N+](=O)[O-]

Technology Process of tert-Butyl (4-nitrobenzoyl)oxycarbamate

There total 3 articles about tert-Butyl (4-nitrobenzoyl)oxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 36016-38-3
tert-Butyl N-hydroxycarbamate

: 62-23-7
4-nitro-benzoic acid

: 35657-41-1
tert-butyl [(4-nitrobenzoyl)oxy]carbamate.

Guidance literature:: With 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide; In dichloromethane; at -10 - 20 ℃;
DOI:10.1016/j.tet.2009.05.007

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 35657-41-1
tert-butyl [(4-nitrobenzoyl)oxy]carbamate.

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; potassium carbonate / diethyl ether; water / 2.25 h / 0 - 20 °C

2: triethylamine / dichloromethane / 1 h / 0 - 20 °C

With hydroxylamine hydrochloride; potassium carbonate; triethylamine; In diethyl ether; dichloromethane; water;