Benzene, (5-hexenylseleno)-

Base Information

Chemical Name:Benzene, (5-hexenylseleno)-
CAS No.:78872-18-1
Molecular Formula:C12H16Se
Molecular Weight:239.219
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, (5-hexenylseleno)-

Chemical Property:

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Technology Process of Benzene, (5-hexenylseleno)-

There total 6 articles about Benzene, (5-hexenylseleno)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 18922-04-8
6-iodohex-1-ene

: 1666-13-3
diphenyl diselenide

: 78872-18-1
5-hexenyl phenyl selenide

Guidance literature:: With zinc; In acetonitrile; for 0.0833333h; pH=14;
DOI:10.1016/j.tetlet.2012.09.063

Reference yield:

: 63668-13-3
Δ⁵-hexenylmercury chloride

: 78872-18-1
5-hexenyl phenyl selenide

Guidance literature:: With PhSeSO₂C₆H₄Me-p; In benzene; byproducts: p-MeC6H4SO2HgCl, cyclopentylcarbinylSePh; Irradiation (UV/VIS); nitrogen atmosphere; mercurial and PhSeSO2C6H4Me-p in deoxygenated solvent irradiated (275-W sunlamp, 35-40 °C, 6h);; filtration; solvent removed (vacuum); yield (detd. by GLC after aq. Na2S2O3/CH2Cl2 extn.) of 5-hexenylSePh and cyclopentylcarbinyl compound: 81%; analysis by (1)H NMR, GLC and GCMS;;
DOI:10.1021/ja00219a030

Reference yield:

: 39179-43-6
(5-hexenyl)2Hg

: 78872-18-1
5-hexenyl phenyl selenide

Guidance literature:: With diphenyl diselenide; In benzene; byproducts: (PhSe)2Hg, cyclopentylcarbinylSePh; Irradiation (UV/VIS); nitrogen atmosphere; mercurial and PhSeSePh (1.2 equiv) in deoxygenated solvent irradiated (275-W sunlamp, 35-40 °C, 4h);; filtration; solvent removed (vacuum); yield (95% of mixt. of 5-hexenyl and cyclopentylcarbinyl compounds) detd. by GLC after aq. Na2S2O3/CH2Cl2 extn.; 5-hexenylSePh analysed by (1)H NMR, GLC and GCMS;;
DOI:10.1021/ja00219a030