2-Cyclopenten-1-one, 3-(3-butenyl)-

Base Information

Chemical Name:2-Cyclopenten-1-one, 3-(3-butenyl)-
CAS No.:79191-35-8
Molecular Formula:C₉H₁₂O
Molecular Weight:136.194
Hs Code.:

Synonyms:

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Chemical Property of 2-Cyclopenten-1-one, 3-(3-butenyl)-

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Technology Process of 2-Cyclopenten-1-one, 3-(3-butenyl)-

There total 1 articles about 2-Cyclopenten-1-one, 3-(3-butenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 130741-35-4
(3-(but-3-enyl)cyclopent-1-enyloxy)trimethylsilane

: 22628-91-7
3-(3-butenyl)cyclopentanone

: 79191-35-8
3-(but-3-en-1-yl)cyclopent-2-en-1-one

: (3aR,6aR)-6-Methyl-3,3a,4,6a-tetrahydro-2H-pentalen-1-one

Guidance literature:: With oxygen; palladium diacetate; In dimethyl sulfoxide; at 45 ℃; under 760.051 Torr;
DOI:10.1021/ol020187u

Reference yield:

: 79191-35-8
3-(but-3-en-1-yl)cyclopent-2-en-1-one

: 6-[(4-methylphenyl)sulfonyl]-1-phenyl-6-azaspiro[4.5]dec-1-ene

Guidance literature:: Multi-step reaction with 6 steps

1.1: 89 percent / NaBH₄; CeCl₃*7H₂O / methanol / 2 h / 0 °C

2.1: 53 percent / PhMe₃NBr₃ / acetonitrile / 18 h / 20 °C

3.1: KHMDS / tetrahydrofuran / 0.5 h / -78 °C

3.2: 73 percent / tetrahydrofuran / 17 h / -78 - 20 °C

4.1: 63 percent / diethyl ether; dibutyl ether / 0.08 h / -78 °C

5.1: 9-BBN / tetrahydrofuran / 0 - 20 °C

5.2: 69 percent / aq. NaOH; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

6.1: 76 percent / PPh₃; DIAD / tetrahydrofuran / 3 h / 20 °C

With sodium tetrahydroborate; 9-borabicyclo[3.3.1]nonane dimer; cerium(III) chloride; di-isopropyl azodicarboxylate; phenyltrimethylammonium tribromide; potassium hexamethylsilazane; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dibutyl ether; acetonitrile; 6.1: Mitsunobu cyclization;
DOI:10.1021/ol062073e

Reference yield:

: 79191-35-8
3-(but-3-en-1-yl)cyclopent-2-en-1-one

: 1-butyl-6-[(4-methylphenyl)sulfonyl]-6-azaspiro[4.5]dec-1-ene

Guidance literature:: Multi-step reaction with 6 steps

1.1: 89 percent / NaBH₄; CeCl₃*7H₂O / methanol / 2 h / 0 °C

2.1: 53 percent / PhMe₃NBr₃ / acetonitrile / 18 h / 20 °C

3.1: KHMDS / tetrahydrofuran / 0.5 h / -78 °C

3.2: 73 percent / tetrahydrofuran / 17 h / -78 - 20 °C

4.1: 80 percent / diethyl ether; hexane / 0.08 h / -78 °C

5.1: 9-BBN / tetrahydrofuran / 0 - 20 °C

5.2: 64 percent / aq. NaOH; aq. H₂O₂ / tetrahydrofuran / 2 h / 20 °C

6.1: 79 percent / PPh₃; DIAD / tetrahydrofuran / 3 h / 20 °C

With sodium tetrahydroborate; 9-borabicyclo[3.3.1]nonane dimer; cerium(III) chloride; di-isopropyl azodicarboxylate; phenyltrimethylammonium tribromide; potassium hexamethylsilazane; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; hexane; acetonitrile; 6.1: Mitsunobu cyclization;
DOI:10.1021/ol062073e