Benzeneacetic acid, 3,5-dichloro-2-(phenylthio)-

Base Information

Chemical Name:Benzeneacetic acid, 3,5-dichloro-2-(phenylthio)-
CAS No.:79332-47-1
Molecular Formula:C14H10Cl2O2S
Molecular Weight:313.204
Hs Code.:
DSSTox Substance ID:DTXSID00356579
Wikidata:Q82135998

Synonyms:Benzeneacetic acid, 3,5-dichloro-2-(phenylthio)-;79332-47-1;DTXSID00356579

Suppliers and Price of Benzeneacetic acid, 3,5-dichloro-2-(phenylthio)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzeneacetic acid, 3,5-dichloro-2-(phenylthio)-

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:311.9778561
Heavy Atom Count:19
Complexity:308

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)SC2=C(C=C(C=C2Cl)Cl)CC(=O)O

Technology Process of Benzeneacetic acid, 3,5-dichloro-2-(phenylthio)-

There total 7 articles about Benzeneacetic acid, 3,5-dichloro-2-(phenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 79332-36-8
<3,5-dichloro-2-(phenylthio)phenyl>acetonitrile

: 79332-47-1
<3,5-dichloro-2-(phenylthio)phenyl>acetic acid

Guidance literature:: With potassium hydroxide; In ethanol; water; for 3h; Heating;
DOI:10.1135/cccc19810781

Reference yield:

: 15396-37-9
2-iodoyl-3,5-dichlorobenzoic acid

: 79332-47-1
<3,5-dichloro-2-(phenylthio)phenyl>acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / K₂CO₃, CuCl / dimethylformamide / 4 h / 140 °C

2: 87 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

3: 96 percent / SOCl₂ / benzene / 1.) 25 deg C, 20 min 2.) 60 deg C, 1 h 3.) reflux 1.5 h

4: 50 percent / dimethylformamide / 2 h / 35 °C

5: 98 percent / KOH / ethanol; H₂O / 3 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; copper(l) chloride; In diethyl ether; ethanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1135/cccc19810781

Reference yield:

: 79332-32-4
3,5-dichloro-2-(phenylthio)benzyl alcohol

: 79332-47-1
<3,5-dichloro-2-(phenylthio)phenyl>acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / SOCl₂ / benzene / 1.) 25 deg C, 20 min 2.) 60 deg C, 1 h 3.) reflux 1.5 h

2: 50 percent / dimethylformamide / 2 h / 35 °C

3: 98 percent / KOH / ethanol; H₂O / 3 h / Heating

With potassium hydroxide; thionyl chloride; In ethanol; water; N,N-dimethyl-formamide; benzene;
DOI:10.1135/cccc19810781