D-Glutamic acid, N-[N-[2-(acetyloxy)-1-oxopropyl]-L-alanyl]-, 1-(phenylmethyl) ester, (R)-, compd. with N-cyclohexylcyclohexanamine (1:1)

Base Information

Chemical Name:D-Glutamic acid, N-[N-[2-(acetyloxy)-1-oxopropyl]-L-alanyl]-, 1-(phenylmethyl) ester, (R)-, compd. with N-cyclohexylcyclohexanamine (1:1)
CAS No.:79390-10-6
Molecular Formula:C₁₂H₂₃N*C₂₀H₂₆N₂O₈
Molecular Weight:603.756
Hs Code.:

Synonyms:

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Chemical Property of D-Glutamic acid, N-[N-[2-(acetyloxy)-1-oxopropyl]-L-alanyl]-, 1-(phenylmethyl) ester, (R)-, compd. with N-cyclohexylcyclohexanamine (1:1)

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Technology Process of D-Glutamic acid, N-[N-[2-(acetyloxy)-1-oxopropyl]-L-alanyl]-, 1-(phenylmethyl) ester, (R)-, compd. with N-cyclohexylcyclohexanamine (1:1)

There total 6 articles about D-Glutamic acid, N-[N-[2-(acetyloxy)-1-oxopropyl]-L-alanyl]-, 1-(phenylmethyl) ester, (R)-, compd. with N-cyclohexylcyclohexanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53636-19-4
(2R)-1-chloro-1-oxopropan-2-yl acetate

: 79390-10-6
(S)-2-[(S)-2-((R)-2-Acetoxy-propionylamino)-propionylamino]-pentanedioic acid 1-benzyl ester; compound with dicyclohexyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: bis(trimethylsilyl)acetamide / CH₂Cl₂ / 1 h / -20 - -10 °C

2: diethyl ether

With bis-(trimethylsilyl)acetamide; In diethyl ether; dichloromethane;
DOI:10.1248/cpb.32.2925

Reference yield:

: 53636-19-4
(2R)-1-chloro-1-oxopropan-2-yl acetate

: 79390-10-6
(R)-2-[(R)-2-((R)-2-Acetoxy-propionylamino)-propionylamino]-pentanedioic acid 1-benzyl ester; compound with dicyclohexyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / bis(trimethylsilyl)acetamide / CH₂Cl₂ / 1 h / -20 - -10 °C

2: diethyl ether

With bis-(trimethylsilyl)acetamide; In diethyl ether; dichloromethane;
DOI:10.1248/cpb.32.2925

Reference yield:

: 60209-60-1
tert-Boc-L-Ala-L-Glu(OH)OBzl

: 79390-10-6
(S)-2-[(S)-2-((R)-2-Acetoxy-propionylamino)-propionylamino]-pentanedioic acid 1-benzyl ester; compound with dicyclohexyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / ethyl acetate

2: bis(trimethylsilyl)acetamide / CH₂Cl₂ / 1 h / -20 - -10 °C

3: diethyl ether

With hydrogenchloride; bis-(trimethylsilyl)acetamide; In diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1248/cpb.32.2925