2-({(E)-[4-(dimethylamino)-3-nitrophenyl]methylidene}amino)-4,5-dimethylthiophene-3-carbonitrile

Base Information

Chemical Name:2-({(E)-[4-(dimethylamino)-3-nitrophenyl]methylidene}amino)-4,5-dimethylthiophene-3-carbonitrile
CAS No.:5309-00-2
Molecular Formula:C₃₅H₅₂O
Molecular Weight:488.797
Hs Code.:
DSSTox Substance ID:DTXSID60430566

Synonyms:5309-00-2;DTXSID60430566;MolPort-002-143-731;STK751934;AKOS001716338;2-({(E)-[4-(dimethylamino)-3-nitrophenyl]methylidene}amino)-4,5-dimethylthiophene-3-carbonitrile;2-({(E)-1-[4-(dimethylamino)-3-nitrophenyl]methylidene}amino)-4,5-dimethyl-3-thienyl cyanide

Suppliers and Price of 2-({(E)-[4-(dimethylamino)-3-nitrophenyl]methylidene}amino)-4,5-dimethylthiophene-3-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-({(E)-[4-(dimethylamino)-3-nitrophenyl]methylidene}amino)-4,5-dimethylthiophene-3-carbonitrile

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:567.7°Cat760mmHg
Flash Point:297.1°C
Density:1.25g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:328.09939694
Heavy Atom Count:23
Complexity:510

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(SC(=C1C#N)N=CC2=CC(=C(C=C2)N(C)C)[N+](=O)[O-])C
Isomeric SMILES:CC1=C(SC(=C1C#N)/N=C/C2=CC(=C(C=C2)N(C)C)[N+](=O)[O-])C

Technology Process of 2-({(E)-[4-(dimethylamino)-3-nitrophenyl]methylidene}amino)-4,5-dimethylthiophene-3-carbonitrile

There total 3 articles about 2-({(E)-[4-(dimethylamino)-3-nitrophenyl]methylidene}amino)-4,5-dimethylthiophene-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 559-74-0
friedelin

: 5309-00-2
2-phenyl-3-oxafriedel-1-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 3.2 g / 39percent peracetic acid / CHCl₃ / 60 °C

2: 2.) sodium acetate / 2.) acetic acid, reflux

3: 300 mg / chromium trioxide / acetic acid / 10 h

4: 650 mg / diethyl ether / 1 h / Heating

With chromium(VI) oxide; peracetic acid; sodium acetate; In diethyl ether; chloroform; acetic acid;
DOI:10.1246/bcsj.60.2117

Reference yield:

: 29621-75-8
3,4-secofriedelan-3 <*> 4-olide

: 5309-00-2
2-phenyl-3-oxafriedel-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) sodium acetate / 2.) acetic acid, reflux

2: 300 mg / chromium trioxide / acetic acid / 10 h

3: 650 mg / diethyl ether / 1 h / Heating

With chromium(VI) oxide; sodium acetate; In diethyl ether; acetic acid;
DOI:10.1246/bcsj.60.2117

Reference yield:

: 113375-98-7
Acetic acid (R)-1-[(1S,2S,4aS,4bR,6aR,10aR,10bS,12aR)-1-(3,3-diphenyl-allyl)-2,4b,6a,9,9,10b,12a-heptamethyl-octadecahydro-chrysen-2-yl]-ethyl ester

: 5309-00-2
2-phenyl-3-oxafriedel-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 300 mg / chromium trioxide / acetic acid / 10 h

2: 650 mg / diethyl ether / 1 h / Heating

With chromium(VI) oxide; In diethyl ether; acetic acid;
DOI:10.1246/bcsj.60.2117