2-Pyridinecarboxylic acid, 6-[[[3-amino-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-oxopropyl][(phen ylmethoxy)carbonyl]amino]methyl]-, methyl ester, (S)-

Base Information

Chemical Name:2-Pyridinecarboxylic acid, 6-[[[3-amino-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-oxopropyl][(phen ylmethoxy)carbonyl]amino]methyl]-, methyl ester, (S)-
CAS No.:80109-37-1
Molecular Formula:C24H30N4O7
Molecular Weight:486.525
Hs Code.:

2-Pyridinecarboxylic acid,
6-[[[3-amino-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-oxopropyl][(phen
ylmethoxy)carbonyl]amino]methyl]-, methyl ester, (S)-

Synonyms:

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Chemical Property of 2-Pyridinecarboxylic acid, 6-[[[3-amino-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-oxopropyl][(phen ylmethoxy)carbonyl]amino]methyl]-, methyl ester, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Pyridinecarboxylic acid, 6-[[[3-amino-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-oxopropyl][(phen ylmethoxy)carbonyl]amino]methyl]-, methyl ester, (S)-

There total 4 articles about 2-Pyridinecarboxylic acid, 6-[[[3-amino-2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-oxopropyl][(phen ylmethoxy)carbonyl]amino]methyl]-, methyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 80109-36-0
methyl 6-<<<(S)-2-<(t-butoxycarbonyl)amino>-2-(carbamoyl)-ethyl>amino>methyl>pyridine-2-carboxylate

: 501-53-1,94274-21-2
benzyl chloroformate

: 80109-37-1
methyl 6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carboxylate

Guidance literature:: With sodium hydroxide; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/0040-4020(84)85055-3

Reference yield:

: 69950-65-8
methyl 6-formylpicolinate

: 80109-37-1
methyl 6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 12 h / 25 °C / activated molecular sieve

2: hydrogen / 5percent Pd-C / methanol

3: 88 percent / 0.1 N NaOH / CH₂Cl₂ / 3 h / 25 °C

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja00413a047

Reference yield:

: 75452-33-4
Boc-Dap(NH₂)-CONH₂

: 80109-37-1
methyl 6-<-2-(carbamoyl)ethyl>amino>methyl>pyridine-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 12 h / 25 °C / activated molecular sieve

2: hydrogen / 5percent Pd-C / methanol

3: 88 percent / 0.1 N NaOH / CH₂Cl₂ / 3 h / 25 °C

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja00413a047