[R,(+)]-2,6-Dimethyl-1,5-heptadien-3-ol

Base Information

Chemical Name:[R,(+)]-2,6-Dimethyl-1,5-heptadien-3-ol
CAS No.:80232-54-8
Molecular Formula:C₁₁H₁₈O₂
Molecular Weight:182.263
Hs Code.:
Mol file:80232-54-8.mol

Synonyms:(R)-(+)-acetoxy-3 dimethyl-2,6 heptadiene-1,5;(R)-(+)-3-Acetoxy-3,6-dimethyl-1,5-heptadiene;Acetic acid (R)-1-isopropenyl-4-methyl-pent-3-enyl ester;

Suppliers and Price of [R,(+)]-2,6-Dimethyl-1,5-heptadien-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of [R,(+)]-2,6-Dimethyl-1,5-heptadien-3-ol

Chemical Property:

Boiling Point:65 - 67 °C (15 mmHg)
PSA：26.30000
LogP:2.85050

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [R,(+)]-2,6-Dimethyl-1,5-heptadien-3-ol

There total 15 articles about [R,(+)]-2,6-Dimethyl-1,5-heptadien-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 80232-52-6
(R)-(+)-dimethyl-2,6 heptadiene-1,5 ol-3

: 108-24-7
acetic anhydride

: 80232-54-8
(R)-(+)-2,6-dimethyl-1,5-heptadien-3-ol acetate

Guidance literature:: With pyridine; for 14h; Ambient temperature;

Reference yield: 50.0%

: 108-24-7
acetic anhydride

: 123731-89-5
(R)-(+)-t-butyldimethylsiloxy-3 dimethyl-2,6 heptadiene-1,5

: 80232-54-8
(R)-(+)-2,6-dimethyl-1,5-heptadien-3-ol acetate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 4h; Heating;

Reference yield:

: 110994-92-8
(R)-(-)-hydroxy-2 methyl-5 hexene-4 oate d'ethyle

: 80232-54-8
(R)-(+)-2,6-dimethyl-1,5-heptadien-3-ol acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / diisopropylethylamine / dimethylformamide / 40 °C

2: 80 percent / TMEDA / diethyl ether; pentane / 4 h / -100 °C

3: 50 percent / n-BuLi / diethyl ether / Ambient temperature

4: 88 percent / pyridinium p-toluenesulfonate / ethanol / 6 h / Heating

5: 90 percent / pyridine / 14 h / Ambient temperature

With pyridine; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; pyridinium p-toluenesulfonate; N-ethyl-N,N-diisopropylamine; In diethyl ether; ethanol; N,N-dimethyl-formamide; pentane;