alpha,6,6-Trimethyl-2-methylenecyclohex-3-ene-1-propan-1-ol

Base Information

Chemical Name:alpha,6,6-Trimethyl-2-methylenecyclohex-3-ene-1-propan-1-ol
CAS No.:57069-87-1
Molecular Formula:C13H22O
Molecular Weight:194.317
Hs Code.:
European Community (EC) Number:260-538-9
DSSTox Substance ID:DTXSID70886217
Nikkaji Number:J349.073D

Synonyms:57069-87-1;alpha,6,6-Trimethyl-2-methylenecyclohex-3-ene-1-propan-1-ol;EINECS 260-538-9;3-Cyclohexene-1-propanol, .alpha.,6,6-trimethyl-2-methylene-;3-Cyclohexene-1-propanol, alpha,6,6-trimethyl-2-methylene-;SCHEMBL11797893;DTXSID70886217;alpha,6,6-Trimethyl-2-methylene-3-cyclohexene-1-(1-propanol)

Suppliers and Price of alpha,6,6-Trimethyl-2-methylenecyclohex-3-ene-1-propan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of alpha,6,6-Trimethyl-2-methylenecyclohex-3-ene-1-propan-1-ol

Chemical Property:

Boiling Point:268.5°Cat760mmHg
Flash Point:98.3°C
Density:0.91g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:194.167065321
Heavy Atom Count:14
Complexity:238

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CCC1C(=C)C=CCC1(C)C)O

Technology Process of alpha,6,6-Trimethyl-2-methylenecyclohex-3-ene-1-propan-1-ol

There total 3 articles about alpha,6,6-Trimethyl-2-methylenecyclohex-3-ene-1-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 79421-96-8
4-(5-Chloro-2,2-dimethyl-6-methylene-cyclohexyl)-butan-2-ol

: 57069-87-1
4-(6,6-Dimethyl-2-methylene-cyclohex-3-enyl)-butan-2-ol

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)92913-2

Reference yield:

: 13720-37-1
dihydro-α-ionol

: 57069-87-1
4-(6,6-Dimethyl-2-methylene-cyclohex-3-enyl)-butan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / NaCl / CH₂Cl₂; H₂O / 4 h / Ambient temperature; electrolysis by using Pt foils at constant current (50 mA)

2: 70 percent / DBU / dimethylformamide

With 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium chloride; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)92913-2