L-Prolinamide, N-[(phenylmethoxy)carbonyl]-D-phenylalanyl-N-[(1S)-1-(2-benzothiazolyl hydroxymethyl)-4-[[imino[[(4-methylphenyl)sulfonyl]amino]methyl]amino] butyl]-

Base Information

Chemical Name:L-Prolinamide, N-[(phenylmethoxy)carbonyl]-D-phenylalanyl-N-[(1S)-1-(2-benzothiazolyl hydroxymethyl)-4-[[imino[[(4-methylphenyl)sulfonyl]amino]methyl]amino] butyl]-
CAS No.:804547-73-7
Molecular Formula:C₄₂H₄₇N₇O₇S₂
Molecular Weight:826.01
Hs Code.:

L-Prolinamide,
N-[(phenylmethoxy)carbonyl]-D-phenylalanyl-N-[(1S)-1-(2-benzothiazolyl
hydroxymethyl)-4-[[imino[[(4-methylphenyl)sulfonyl]amino]methyl]amino]
butyl]-

Synonyms:

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Chemical Property of L-Prolinamide, N-[(phenylmethoxy)carbonyl]-D-phenylalanyl-N-[(1S)-1-(2-benzothiazolyl hydroxymethyl)-4-[[imino[[(4-methylphenyl)sulfonyl]amino]methyl]amino] butyl]-

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Technology Process of L-Prolinamide, N-[(phenylmethoxy)carbonyl]-D-phenylalanyl-N-[(1S)-1-(2-benzothiazolyl hydroxymethyl)-4-[[imino[[(4-methylphenyl)sulfonyl]amino]methyl]amino] butyl]-

There total 1 articles about L-Prolinamide, N-[(phenylmethoxy)carbonyl]-D-phenylalanyl-N-[(1S)-1-(2-benzothiazolyl hydroxymethyl)-4-[[imino[[(4-methylphenyl)sulfonyl]amino]methyl]amino] butyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 179746-24-8
C₂₀H₂₅N₅O₃S₂*C₂HF₃O₂

: 17460-56-9
N-[[(Phenylmethoxy)-carbonyl]-D-phenylalanyl]-L-proline

: 804547-73-7
C₄₂H₄₇N₇O₇S₂

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; triethylamine; dicyclohexyl-carbodiimide; In acetonitrile; for 18h; pH=7 - 8;
DOI:10.1021/jm0303857

Reference yield:

: 804547-73-7
C₄₂H₄₇N₇O₇S₂

: C₄₂H₄₅N₇O₇S₂

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 2h;
DOI:10.1021/jm0303857

Reference yield:

: 804547-73-7
C₄₂H₄₇N₇O₇S₂

: (S)-1-((R)-2-Amino-3-phenyl-propionyl)-pyrrolidine-2-carboxylic acid [1-(benzothiazole-2-carbonyl)-4-guanidino-butyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodinane / CH₂Cl₂ / 2 h

2: HF; anisole / -78 - 5 °C

With hydrogen fluoride; Dess-Martin periodane; methoxybenzene; In dichloromethane; 1: Dess-Martin oxidation;
DOI:10.1021/jm0303857