Technology Process of 5-oxo-5,13-dihydrodibenzo[c,g][1,5,6]oxadiazonin-5-ium-6(11H)-olate
There total 6 articles about 5-oxo-5,13-dihydrodibenzo[c,g][1,5,6]oxadiazonin-5-ium-6(11H)-olate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tungstate (VI) dihydrate; dihydrogen peroxide;
In
ethanol; water;
at 20 ℃;
for 24h;
DOI:10.3987/COM-10-12065
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 11.39 g / silver oxide / dimethylformamide / overnight
2: 93 percent / 85percent hydrazine hydrate, hydrogen / Pd/C / ethanol / 1.) 15 min, room temp.; 2.) reflux, 1 h
3: 20.5 percent / sodium tungstate dihydrate, 30percent hydrogen peroxide / ethanol; H2O / 24 h / Ambient temperature
With
sodium tungstate; hydrogen; dihydrogen peroxide; hydrazine hydrate; silver(l) oxide;
palladium on activated charcoal;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo01311a009
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 93 percent / 85percent hydrazine hydrate, hydrogen / Pd/C / ethanol / 1.) 15 min, room temp.; 2.) reflux, 1 h
2: 20.5 percent / sodium tungstate dihydrate, 30percent hydrogen peroxide / ethanol; H2O / 24 h / Ambient temperature
With
sodium tungstate; hydrogen; dihydrogen peroxide; hydrazine hydrate;
palladium on activated charcoal;
In
ethanol; water;
DOI:10.1021/jo01311a009
