1-(9-Chlorononyl)-4-nitrosobenzene

Base Information

Chemical Name:1-(9-Chlorononyl)-4-nitrosobenzene
CAS No.:81815-23-8
Molecular Formula:C15H22ClNO
Molecular Weight:267.799
Hs Code.:
DSSTox Substance ID:DTXSID10510382
Wikidata:Q82368627

Synonyms:1-(9-CHLORONONYL)-4-NITROSOBENZENE;81815-23-8;SCHEMBL10955926;DTXSID10510382

Suppliers and Price of 1-(9-Chlorononyl)-4-nitrosobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-(9-Chlorononyl)-4-nitrosobenzene

Chemical Property:

XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:9
Exact Mass:267.1389920
Heavy Atom Count:18
Complexity:203

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1CCCCCCCCCCl)N=O

Technology Process of 1-(9-Chlorononyl)-4-nitrosobenzene

There total 1 articles about 1-(9-Chlorononyl)-4-nitrosobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81815-22-7
1-chloro-9-phenyl>nonane

: 81815-23-8
1-chloro-9-(p-nitrosophenyl)nonane

Guidance literature:: With hydrogenchloride; isopentyl nitrite; In dichloromethane; for 0.333333h; Yield given; Ambient temperature;
DOI:10.1021/jo00136a040

Reference yield: 97.0%

: 81815-23-8
1-chloro-9-(p-nitrosophenyl)nonane

: 81830-39-9
1-chloro-9-(p-aminophenyl)nonane

Guidance literature:: With sodium tetrahydroborate; palladium on activated charcoal; In methanol; for 0.5h; Ambient temperature;
DOI:10.1021/jo00136a040

Reference yield:

: 81815-23-8
1-chloro-9-(p-nitrosophenyl)nonane

: 81815-25-0
1-chloro-9-(p-iodophenyl)nonane

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaBH₄ / 10percent Pd/C / methanol / 0.5 h / Ambient temperature

2: 1.) NaNO₂, 0.5 N HCl / 1.) 0-5 deg C, 5 min, 2.) 0-5 deg C, 30 min

3: 60 percent / NaI, CF₃CO₂H / acetone / 0.08 h / 0 - 5 °C

With hydrogenchloride; sodium tetrahydroborate; trifluoroacetic acid; sodium iodide; sodium nitrite; palladium on activated charcoal; In methanol; acetone;
DOI:10.1021/jo00136a040