1(2H)-Azocineacetic acid, 3-[(1-carboxy-3-phenylpropyl)amino]hexahydro-2-oxo-

Base Information

Chemical Name:1(2H)-Azocineacetic acid, 3-[(1-carboxy-3-phenylpropyl)amino]hexahydro-2-oxo-
CAS No.:81867-08-5
Molecular Formula:C₁₉H₂₆N₂O₅
Molecular Weight:362.426
Hs Code.:

Synonyms:

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Chemical Property of 1(2H)-Azocineacetic acid, 3-[(1-carboxy-3-phenylpropyl)amino]hexahydro-2-oxo-

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Technology Process of 1(2H)-Azocineacetic acid, 3-[(1-carboxy-3-phenylpropyl)amino]hexahydro-2-oxo-

There total 12 articles about 1(2H)-Azocineacetic acid, 3-[(1-carboxy-3-phenylpropyl)amino]hexahydro-2-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32566-61-3
3-bromohexahydroazocin-2(1H)-one

: 81867-08-5,81874-34-2,99707-59-2,99707-60-5,99707-61-6,99781-14-3,99781-15-4
(+/-)-1-(carboxymethyl)-3-<(1-carboxy-3-phenylpropyl)amino>perhydroazocin-2-one

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / sodium azide / ethanol; H₂O

2: 76 percent / NaH / tetrahydrofuran / 1.5 h / Heating

3: 100 percent / H₂ / 10percent Pd/C

4: 16 percent / acetic cid, H₂ / 10percent Pd/C / ethanol / 2068.6 Torr / Ambient temperature

5: 2 h / Ambient temperature

6: NaOH / methanol / Ambient temperature

With sodium hydroxide; sodium azide; hydrogen; sodium hydride; acetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; water;
DOI:10.1021/jm00152a014

Reference yield:

: 32566-61-3
3-bromohexahydroazocin-2(1H)-one

: 81867-08-5,81874-34-2,99707-59-2,99707-60-5,99707-61-6,99781-14-3,99781-15-4
(+/-)-1-(carboxymethyl)-3-<(1-carboxy-3-phenylpropyl)amino>perhydroazocin-2-one

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / sodium azide / ethanol; H₂O

2: 76 percent / NaH / tetrahydrofuran / 1.5 h / Heating

3: 100 percent / H₂ / 10percent Pd/C

4: 35 percent / acetic cid, H₂ / 10percent Pd/C / ethanol / 2068.6 Torr / Ambient temperature

5: 2 h / Ambient temperature

6: 1 N NaOH / methanol / Ambient temperature

With sodium hydroxide; sodium azide; hydrogen; sodium hydride; acetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; water;
DOI:10.1021/jm00152a014

Reference yield:

: 81867-12-1
3-azidohexahydro-2(1H)-azocinone

: 81867-08-5,81874-34-2,99707-59-2,99707-60-5,99707-61-6,99781-14-3,99781-15-4
(+/-)-1-(carboxymethyl)-3-<(1-carboxy-3-phenylpropyl)amino>perhydroazocin-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / NaH / tetrahydrofuran / 1.5 h / Heating

2: 100 percent / H₂ / 10percent Pd/C

3: 16 percent / acetic cid, H₂ / 10percent Pd/C / ethanol / 2068.6 Torr / Ambient temperature

4: 2 h / Ambient temperature

5: NaOH / methanol / Ambient temperature

With sodium hydroxide; hydrogen; sodium hydride; acetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00152a014