Benzene, 1-chloro-4-(methoxymethoxy)-

Base Information

• Chemical Name: Benzene, 1-chloro-4-(methoxymethoxy)-
• CAS No.: 826-26-6
• Molecular Formula: C8H9ClO2
• Molecular Weight: 172.611
• Hs Code.: 2909309090

Synonyms:Methyl-p-chlorphenyl-formal;4-Chlor-methoxymethoxybenzol;1-methoxymethoxy-4-chlorobenzene;(4-Chlor-phenoxy)-methoxy-methan;

Chemical Property of Benzene, 1-chloro-4-(methoxymethoxy)-

Chemical Property:

• PSA: 18.46000
• LogP: 2.32270

Purity/Quality:

99% ^*data from raw suppliers

4-Chloro-1-(methoxymethoxy)benzene 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzene, 1-chloro-4-(methoxymethoxy)-

There total 3 articles about Benzene, 1-chloro-4-(methoxymethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

Dimethoxymethane (109-87-5) + 4-chloro-phenol (106-48-9,82344-39-6) → 1-chloro-4-(methoxymethoxy)benzene (826-26-6)

Guidance literature:

With zirconyl triflate; at 20 ℃; for 0.166667h; chemoselective reaction; neat (no solvent);

DOI:10.1007/s00706-010-0310-8

Reference yield:

chloromethyl methyl ether (107-30-2) + 4-chloro-phenol (106-48-9,82344-39-6) → 1-chloro-4-(methoxymethoxy)benzene (826-26-6)

Guidance literature:

With sodium hydride; In benzene;

DOI:10.1021/ja00751a025

Reference yield:

→ 1-chloro-4-(methoxymethoxy)benzene (826-26-6)

Guidance literature:

Chlormethyl-methylether, p-Chlorphenol-Na (in DMSO);

upstream raw materials:

chloromethyl methyl ether

4-chloro-phenol

Dimethoxymethane

Downstream raw materials:

2-(methoxymethoxy)-5-chlorobenzaldehyde

4-bromo-2-[5-chloro-2-(methoxymethoxy)phenyl]thiazole

2-methoxymethoxy-5-chlorophenylboronic acid

5-Chloro-2-methoxymethoxy-benzoic acid

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