Tungsten, dichlorotetrakis(4-methylphenolato)-

Base Information

Chemical Name:Tungsten, dichlorotetrakis(4-methylphenolato)-
CAS No.:82972-36-9
Molecular Formula:C28H28Cl2O4W
Molecular Weight:683.284
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tungsten, dichlorotetrakis(4-methylphenolato)-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Tungsten, dichlorotetrakis(4-methylphenolato)-

There total 1 articles about Tungsten, dichlorotetrakis(4-methylphenolato)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 106-44-5
p-cresol

: 13283-01-7
tungsten(VI) chloride

: 82972-36-9
tungsten(VI)(4-methylphenoxide)4-dichloride

Guidance literature:: In tetrachloromethane; addn. of soln. of 4-CH3C6H4OH in CCl4 to WCl6 suspended in CCl4 (Ar-atmosphere); stirring under reflux for 1 h;; evapn. and chromy. on silica gel column (toluene/hexane 50/50); crystn. at -5°C; elem. anal.;;

Reference yield:

: 106-44-5
p-cresol

: 82972-36-9
tungsten(VI)(4-methylphenoxide)4-dichloride

: 4503-99-5
hexa(p-methylphenoxy)tungsten

Guidance literature:: In benzene; W-compound and 4-methylphenol were mixed in benzene and refluxed for 12 h; solvent was removed and prod. was heated in vac. at 80-90°C;