3,3-Dimethyl-4-(dimethylamino)-4-(o-methoxyphenyl)butyl o-methoxyphenyl ketone

Base Information

• Chemical Name: 3,3-Dimethyl-4-(dimethylamino)-4-(o-methoxyphenyl)butyl o-methoxyphenyl ketone
• CAS No.: 3215-85-8
• Molecular Formula: C₂₃H₃₁NO₃
• Molecular Weight: 369.504
• DSSTox Substance ID: DTXSID50954009
• Nikkaji Number: J41.548K
• Mol file: 3215-85-8.mol

Synonyms:BRN 2821940;3215-85-8;3,3-Dimethyl-4-(dimethylamino)-4-(o-methoxyphenyl)butyl o-methoxyphenyl ketone;KETONE, 3,3-DIMETHYL-4-(DIMETHYLAMINO)-4-(o-METHOXYPHENYL)BUTYL o-METHOXYPHENYL;DTXSID50954009;5-(dimethylamino)-1,5-bis(2-methoxyphenyl)-4,4-dimethylpentan-1-one;LS-87179;omega-(Dimethylamino)-2'-methoxy-omega-(o-methoxyphenyl)-gamma,gamma-dimethylvalerophenone;Valerophenone, 5-(dimethylamino)-2'-methoxy-5-(o-methoxyphenyl)-4,4-dimethyl-

Chemical Property of 3,3-Dimethyl-4-(dimethylamino)-4-(o-methoxyphenyl)butyl o-methoxyphenyl ketone

Chemical Property:

• Vapor Pressure: 6.4E-10mmHg at 25°C
• Boiling Point: 494.5°Cat760mmHg
• Flash Point: 252.9°C
• Density: 1.045g/cm³
• XLogP3: 4.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 9
• Exact Mass: 369.23039385
• Heavy Atom Count: 27
• Complexity: 463

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(CCC(=O)C1=CC=CC=C1OC)C(C2=CC=CC=C2OC)N(C)C

Technology Process of 3,3-Dimethyl-4-(dimethylamino)-4-(o-methoxyphenyl)butyl o-methoxyphenyl ketone

There total 2 articles about 3,3-Dimethyl-4-(dimethylamino)-4-(o-methoxyphenyl)butyl o-methoxyphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-(dimethylamino)-3,3-dimethylcyclobutane-carboxylate (3854-82-8) + 2-methoxyphenylmagnesium bromide (16750-63-3) → 1,5-Di-(o-methoxy-phenyl)-4,4-dimethyl-5-dimethylamino-pentanon-(1) (3215-85-8)

Guidance literature:

In diethyl ether;

DOI:10.1021/ja01076a031 DOI:10.1021/jm00320a007

Reference yield:

→ 1,5-Di-(o-methoxy-phenyl)-4,4-dimethyl-5-dimethylamino-pentanon-(1) (3215-85-8)

Guidance literature:

Methyl-2-dimethylamino-3,3-dimethylcyclobutancarboxylat, o-Methoxyphenyl-Mg-Br;

upstream raw materials:

methyl 2-(dimethylamino)-3,3-dimethylcyclobutane-carboxylate

2-methoxyphenylmagnesium bromide

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