Carbamic acid, 8-azabicyclo[3.2.1]oct-3-yl-, ethyl ester, exo-

Base Information

Chemical Name:Carbamic acid, 8-azabicyclo[3.2.1]oct-3-yl-, ethyl ester, exo-
CAS No.:83791-16-6
Molecular Formula:C10H18N2O2
Molecular Weight:
Hs Code.:

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Chemical Property of Carbamic acid, 8-azabicyclo[3.2.1]oct-3-yl-, ethyl ester, exo-

Chemical Property:

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Technology Process of Carbamic acid, 8-azabicyclo[3.2.1]oct-3-yl-, ethyl ester, exo-

There total 4 articles about Carbamic acid, 8-azabicyclo[3.2.1]oct-3-yl-, ethyl ester, exo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 83791-13-3
8-Benzyl-3β-(N-carbethoxy)amino-1αH,5αH-nortropane

: 83791-16-6
3β-(N-Carbethoxy)amino-1αH,5αH-nortropane

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; for 24h; under 1802 Torr; Ambient temperature;
DOI:10.1002/jhet.5570190307

Reference yield:

: 76272-36-1
8-benzyl-8-aza-bicyclo[3.2.1]oct-3-yl-amine

: 83791-16-6
3β-(N-Carbethoxy)amino-1αH,5αH-nortropane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Anhydrous sodium carbonate / acetonitrile / 1.) 0 deg C, 2.) reflux, 16 h

2: 77 percent / Hydrogen, Acetic acid / 10percent Palladium-on-carbon / ethanol / 24 h / 1802 Torr / Ambient temperature

With hydrogen; sodium carbonate; acetic acid; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1002/jhet.5570190307

Reference yield:

: 28957-72-4
N-benzylnortropinone

: 83791-16-6
3β-(N-Carbethoxy)amino-1αH,5αH-nortropane

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / Hydroxylamine hydrochloride, sodium bicarbonate / aq. ethanol / 0.5 h / 100 °C

2: 66 percent / Sodium, ethanol / 16 h / Heating

3: 75 percent / Anhydrous sodium carbonate / acetonitrile / 1.) 0 deg C, 2.) reflux, 16 h

4: 77 percent / Hydrogen, Acetic acid / 10percent Palladium-on-carbon / ethanol / 24 h / 1802 Torr / Ambient temperature

With ethanol; hydroxylamine hydrochloride; hydrogen; sodium; sodium hydrogencarbonate; sodium carbonate; acetic acid; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1002/jhet.5570190307