3,9-Dimethylfluorene

Base Information

Chemical Name:3,9-Dimethylfluorene
CAS No.:96563-07-4
Molecular Formula:C₁₅H₁₄
Molecular Weight:194.276
Hs Code.:
DSSTox Substance ID:DTXSID20914453
Mol file:96563-07-4.mol

Synonyms:3,9-Dimethylfluorene;96563-07-4;CCRIS 4268;3,9-dimethyl-9H-fluorene;9H-Fluorene, 3,9-dimethyl-;DTXSID20914453

Suppliers and Price of 3,9-Dimethylfluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3,9-Dimethylfluorene

Chemical Property:

Vapor Pressure:0.000655mmHg at 25°C
Boiling Point:318.9°Cat760mmHg
Flash Point:152.7°C
PSA：0.00000
Density:1.052g/cm³
LogP:4.12720
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:194.109550447
Heavy Atom Count:15
Complexity:232

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1C2=C(C=C(C=C2)C)C3=CC=CC=C13

Technology Process of 3,9-Dimethylfluorene

There total 2 articles about 3,9-Dimethylfluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₂N₂O₂S

: 17057-98-6
1,9-dimethyl-9H-fluorene

: 96563-07-4
3,9-dimethyl-9H-fluorene

Guidance literature:: With sodium hydride; In toluene; at 110 ℃; for 15h; Overall yield = 99 %; Inert atmosphere;
DOI:10.1002/anie.201409982

Reference yield:

: 893739-26-9
1-(3′-methyl-[1,1′-biphenyl]-2-yl)ethanone

: 17057-98-6
1,9-dimethyl-9H-fluorene

: 96563-07-4
3,9-dimethyl-9H-fluorene

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 110 °C / Inert atmosphere

2: sodium hydride / toluene / 15 h / 110 °C / Inert atmosphere

With sodium hydride; In ethanol; toluene;
DOI:10.1002/anie.201409982