Thiophene, 3,3'-thiobis-

Base Information

Chemical Name:Thiophene, 3,3'-thiobis-
CAS No.:3807-38-3
Molecular Formula:C8H6S3
Molecular Weight:198.334
Hs Code.:
DSSTox Substance ID:DTXSID70191479
Nikkaji Number:J1.853.680C
Wikidata:Q83064000
Mol file:3807-38-3.mol

Synonyms:Thiophene, 3,3'-thiobis-;3807-38-3;Di(thiophen-3-yl)sulfane;3-thiophen-3-ylsulfanylthiophene;Di-(3-thienyl)sulfide;Thiophene,3,3'-thiobis-;di(3-thienyl)sulfide;3,3'-Thiobisthiophene;SCHEMBL6665571;3-(3-Thienylsulfanyl)thiophene;DTXSID70191479;3-(3-Thienylsulfanyl)thiophene #

Suppliers and Price of Thiophene, 3,3'-thiobis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Thiophene, 3,3'-thiobis-

Chemical Property:

Boiling Point:315°Cat760mmHg
Flash Point:144.3°C
Density:1.37g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:197.96316371
Heavy Atom Count:11
Complexity:113

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CSC=C1SC2=CSC=C2

Technology Process of Thiophene, 3,3'-thiobis-

There total 1 articles about Thiophene, 3,3'-thiobis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 96-43-5
2-thienyl chloride

: 188290-36-0,8014-23-1,25233-34-5
thiophene

: 7774-74-5
Thiophene-2-thiol

: 7774-73-4
thiophene-3-thiol

: 3807-38-3
sulfure de dithienyle-3,3'

: 3807-37-2
2-thienyl 3-thienyl sulfide

: 3988-99-6
bis(thien-2-yl)sulfide

Guidance literature:: With dimethylselenide; hydrogen sulfide; In gas; at 500 ℃; Product distribution; Mechanism; effect of dimethyl selenide on reaction; various temperatures;

Reference yield: 48.0%

: 3807-38-3
sulfure de dithienyle-3,3'

: 34907-53-4
dimethoxy(mesityl)borane

: C₁₇H₁₅BS₃

Guidance literature:: sulfure de dithienyle-3,3'; With n-butyllithium; In diethyl ether; hexane; at -3 - 40 ℃; for 2.5h; Inert atmosphere;

dimethoxy(mesityl)borane; In diethyl ether; hexane;

Reference yield:

: 3807-38-3
sulfure de dithienyle-3,3'

: C₂₆H₂₈S₅Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / diethyl ether / 1 h / 0 - 40 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: acetic acid; N-Bromosuccinimide / chloroform / 3 h / 0 - 20 °C

3.1: n-butyllithium; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide / tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere

4.1: n-butyllithium / diethyl ether / 0.5 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; acetic acid; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; chloroform;
DOI:10.1002/anie.201410970