Technology Process of 2,3,4,5-Tetrabromo-6-methyl-6-nitrocyclohexa-2,4-dien-1-one
There total 3 articles about 2,3,4,5-Tetrabromo-6-methyl-6-nitrocyclohexa-2,4-dien-1-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 81 percent / Br2 / iron / CCl4 / 1.) 5 h bromine introduction; 2.) 24 h room temp.
2: 52 percent / nitric acid / acetic acid / 1.) 10 min 10 deg C; 2.) 2 h 5 deg C
With
bromine; nitric acid;
iron;
In
tetrachloromethane; acetic acid;
DOI:10.1016/S0040-4020(01)90020-1
- Guidance literature:
-
With
nitric acid;
In
acetic acid;
at 0 ℃;