N-Allyl-2-allylthio-2-ethylbutyramide

Base Information

• Chemical Name: N-Allyl-2-allylthio-2-ethylbutyramide
• CAS No.: 66859-77-6
• Molecular Formula: C12H21NOS
• Molecular Weight: 227.3662
• Mol file: 66859-77-6.mol

Synonyms:2-Allylmercapto-2-aethyl-buttersaeure-allylamid;BUTYRAMIDE,N-ALLYL-2-ALLYLTHIO-2-ETHYL;2-Aethyl-N-allyl-2-allylmercapto-butyramid;2-Aethyl-2-allylmercapto-buttersaeure-allylamid;N-Allyl-2-allylthio-2-ethylbutyramide;2-ethyl-2-allylmercapto-butyric acid allylamide;

Chemical Property of N-Allyl-2-allylthio-2-ethylbutyramide

Chemical Property:

• Vapor Pressure: 2.61E-05mmHg at 25°C
• Boiling Point: 358.1°Cat760mmHg
• Flash Point: 170.4°C
• PSA: 57.89000
• Density: 0.96g/cm³
• LogP: 3.60690

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-Allyl-2-allylthio-2-ethylbutyramide

There total 3 articles about N-Allyl-2-allylthio-2-ethylbutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-mercapto-2-ethylbutyric acid (52988-77-9) → 2-Allylmercapto-2-aethyl-buttersaeure-allylamid (66859-77-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium ethylate; ethanol / anschliessendes Behandeln mit Allylbromid

2: thionyl chloride

3: diethyl ether

With thionyl chloride; diethyl ether; ethanol; sodium ethanolate;

Reference yield:

2-ethyl-2-allylmercapto-butyric acid (90646-84-7) → 2-Allylmercapto-2-aethyl-buttersaeure-allylamid (66859-77-6)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride

2: diethyl ether

With thionyl chloride; diethyl ether;

Reference yield:

2-ethyl-2-allylmercapto-butyryl chloride (90722-39-7) + 1-amino-2-propene (107-11-9,30551-89-4) → 2-Allylmercapto-2-aethyl-buttersaeure-allylamid (66859-77-6)

Guidance literature:

With diethyl ether;

upstream raw materials:

2-ethyl-2-allylmercapto-butyryl chloride

1-amino-2-propene

2-mercapto-2-ethylbutyric acid

2-ethyl-2-allylmercapto-butyric acid

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