Ethanone, 1-phenyl-, (5-((2-chlorophenyl)amino)-1,3,4-thiadiazol-2-yl)hydrazone, (1E)-

Base Information

Chemical Name:Ethanone, 1-phenyl-, (5-((2-chlorophenyl)amino)-1,3,4-thiadiazol-2-yl)hydrazone, (1E)-
CAS No.:127142-30-7
Molecular Formula:C15H13 Cl N6 S
Molecular Weight:343.8339
Hs Code.:
Mol file:127142-30-7.mol

Synonyms:Ethanone, 1-phenyl-, (5-((2-chlorophenyl)amino)-1,3,4-thiadiazol-2-yl)hydrazone, (1E)-;Ethanone, 1-phenyl-, [5-[(2-chlorophenyl)amino]-1,3,4-thiadiazol-2-yl]hydrazone, (1E)-;N5-(2-chlorophenyl)-N2-[(E)-1-phenylethylideneamino]-1,3,4-thiadiazole-2,5-diamine

Suppliers and Price of Ethanone, 1-phenyl-, (5-((2-chlorophenyl)amino)-1,3,4-thiadiazol-2-yl)hydrazone, (1E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Ethanone, 1-phenyl-, (5-((2-chlorophenyl)amino)-1,3,4-thiadiazol-2-yl)hydrazone, (1E)-

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:496°Cat760mmHg
Flash Point:253.8°C
Density:1.36g/cm³
XLogP3:5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:343.0658443
Heavy Atom Count:23
Complexity:402

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NNC1=NN=C(S1)NC2=CC=CC=C2Cl)C3=CC=CC=C3
Isomeric SMILES:C/C(=N\NC1=NN=C(S1)NC2=CC=CC=C2Cl)/C3=CC=CC=C3

Technology Process of Ethanone, 1-phenyl-, (5-((2-chlorophenyl)amino)-1,3,4-thiadiazol-2-yl)hydrazone, (1E)-

There total 3 articles about Ethanone, 1-phenyl-, (5-((2-chlorophenyl)amino)-1,3,4-thiadiazol-2-yl)hydrazone, (1E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 127142-14-7
2-acetylpyridine 5-<(2-chloroanilino)thiocarbonyl>thiocarbonohydrazone

: 127142-30-7
N-(2-chlorophenyl)-5-(2-(1-(pyridin-2-yl)ethylidene)hydrazinyl)-1,3,4-thiadiazol-2-amine

Guidance literature:: With tert.-butylhydroperoxide; triethylamine; In methanol; for 1.25h; Ambient temperature;
DOI:10.1021/jm00090a022

Reference yield:

: 1122-62-9
2-acetylpyridine

: 127142-30-7
N-(2-chlorophenyl)-5-(2-(1-(pyridin-2-yl)ethylidene)hydrazinyl)-1,3,4-thiadiazol-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / methanol / Heating

2: 79 percent / dimethylformamide / 0.5 h / Ambient temperature

3: 85 percent / 90percent tert-butyl hydroperoxide, Et₃N / methanol / 1.25 h / Ambient temperature

With tert.-butylhydroperoxide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00090a022

Reference yield:

: 96699-87-5
methyl 2-pyridyl ketone thiocarbonohydrazone

: 127142-30-7
N-(2-chlorophenyl)-5-(2-(1-(pyridin-2-yl)ethylidene)hydrazinyl)-1,3,4-thiadiazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / dimethylformamide / 0.5 h / Ambient temperature

2: 85 percent / 90percent tert-butyl hydroperoxide, Et₃N / methanol / 1.25 h / Ambient temperature

With tert.-butylhydroperoxide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00090a022