1H-Pyrazole-4-pentanoic acid

Base Information

Chemical Name:1H-Pyrazole-4-pentanoic acid
CAS No.:84302-88-5
Molecular Formula:C₈H₁₂N₂O₂
Molecular Weight:168.195
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Pyrazole-4-pentanoic acid

Chemical Property:

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Technology Process of 1H-Pyrazole-4-pentanoic acid

There total 8 articles about 1H-Pyrazole-4-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 84302-85-2
4-(4-pyrazolyl)pentanenitrile

: 84302-88-5
4-(4-pyrazolyl)pentanoic acid

Guidance literature:: With sulfuric acid; for 2.5h; Heating;

Reference yield:

: 84302-83-0
4-(3-chloropropyl)pyrazole

: 84302-88-5
4-(4-pyrazolyl)pentanoic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 72 percent / dimethylsulfoxide / 2.5 h / Heating

2: 91 percent / HCl gas / 0 deg C, 2 h, room temp. overnight

3: 86 percent / water / 40 deg C, 15 min, room temp. overnight

4: 47 percent / LiAlH₄ / diethyl ether / 6 h / Heating

5: thionyl chloride / benzene / 1 h / Heating

6: 90 percent / dimethylsulfoxide / 2.5 h / Heating

7: 68 percent / 65percent H₂SO₄ / 2.5 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; sulfuric acid; water; In diethyl ether; dimethyl sulfoxide; benzene;

Reference yield:

: 60951-21-5
3-(1H-pyrazol-4-yl)propan-1-ol

: 84302-88-5
4-(4-pyrazolyl)pentanoic acid

Guidance literature:: Multi-step reaction with 8 steps

1: thionyl chloride / benzene / 1 h / Heating

2: 72 percent / dimethylsulfoxide / 2.5 h / Heating

3: 91 percent / HCl gas / 0 deg C, 2 h, room temp. overnight

4: 86 percent / water / 40 deg C, 15 min, room temp. overnight

5: 47 percent / LiAlH₄ / diethyl ether / 6 h / Heating

6: thionyl chloride / benzene / 1 h / Heating

7: 90 percent / dimethylsulfoxide / 2.5 h / Heating

8: 68 percent / 65percent H₂SO₄ / 2.5 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; sulfuric acid; water; In diethyl ether; dimethyl sulfoxide; benzene;