2-(Benzenesulfonyl)hex-1-en-3-ol

Base Information

Chemical Name:2-(Benzenesulfonyl)hex-1-en-3-ol
CAS No.:84363-80-4
Molecular Formula:C12H16O3S
Molecular Weight:240.31900
Hs Code.:
DSSTox Substance ID:DTXSID70510080

Synonyms:2-(Benzenesulfonyl)hex-1-en-3-ol;84363-80-4;DTXSID70510080;2-(phenylsulfonyl)-1-hexen-3-ol;2-(benzenesulfonyl)-hex-1-en-3-ol

Suppliers and Price of 2-(Benzenesulfonyl)hex-1-en-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(Benzenesulfonyl)hex-1-en-3-ol

Chemical Property:

PSA：62.75000
LogP:3.21580
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:240.08201554
Heavy Atom Count:16
Complexity:321

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC(C(=C)S(=O)(=O)C1=CC=CC=C1)O

Technology Process of 2-(Benzenesulfonyl)hex-1-en-3-ol

There total 6 articles about 2-(Benzenesulfonyl)hex-1-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 5535-48-8
PVS

: 123-72-8
butyraldehyde

: 84363-80-4
2-(Benzenesulfonyl)-1-hexen-3-ol

Guidance literature:: 1,4-diaza-bicyclo[2.2.2]octane; at 25 ℃;
DOI:10.1016/S0040-4039(00)85142-4

Reference yield:

: 84363-76-8
2-Benzenesulfonyl-2-chloro-1-trimethylsilanyl-hexan-3-ol

: 84363-80-4
2-(Benzenesulfonyl)-1-hexen-3-ol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 0.166667h; Yield given;
DOI:10.1016/S0040-4039(00)87640-6

Reference yield:

: 73476-18-3
1-benzenesulfonyl-2-trimethylsilylethane

: 84363-80-4
2-(Benzenesulfonyl)-1-hexen-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1: n-butyllithium / hexane; diethyl ether / -70 °C

2: 97 percent / CrO₃, H₂SO₄ / acetone / 1 h / 0 - 5 °C

3: 99 percent / KOH, NaOCl / dioxane / 2.5 h

4: n-butyllithium / hexane; diethyl ether / 0.5 h / -70 °C

5: tetra-n-butylammonium fluoride / tetrahydrofuran / 0.17 h / 25 °C

With chromium(VI) oxide; potassium hydroxide; sodium hypochlorite; n-butyllithium; sulfuric acid; tetrabutyl ammonium fluoride; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; acetone;
DOI:10.1016/S0040-4039(00)87640-6