(5Z)-4-(4-chlorophenyl)-5-[(4-chlorophenyl)imino]-1,2,4-dithiazolidine-3-thione

Base Information

• Chemical Name: (5Z)-4-(4-chlorophenyl)-5-[(4-chlorophenyl)imino]-1,2,4-dithiazolidine-3-thione
• CAS No.: 23509-92-4
• Molecular Formula: C14H8 Cl2 N2 S3
• Molecular Weight: 371.3277
• Mol file: 23509-92-4.mol

Synonyms:1,2,4-Dithiazolidine-3-thione,4-(p-chlorophenyl)-5-[(p-chlorophenyl)imino]- (8CI)

Chemical Property of (5Z)-4-(4-chlorophenyl)-5-[(4-chlorophenyl)imino]-1,2,4-dithiazolidine-3-thione

Chemical Property:

• Vapor Pressure: 2.7E-10mmHg at 25°C
• Boiling Point: 504.3°Cat760mmHg
• Flash Point: 258.8°C
• Density: 1.51g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (5Z)-4-(4-chlorophenyl)-5-[(4-chlorophenyl)imino]-1,2,4-dithiazolidine-3-thione

There total 4 articles about (5Z)-4-(4-chlorophenyl)-5-[(4-chlorophenyl)imino]-1,2,4-dithiazolidine-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride (5180-19-8) + p-chlorophenyldithiocarbamic acid triethylamine salt (43009-19-4) → 4-(4-chloro-phenyl)-5-(4-chloro-phenylimino)-[1,2,4]dithiazolidine-3-thione (23509-92-4)

Guidance literature:

In benzene; Ambient temperature;

Reference yield: 9.0%

S-chloro-N-phenylisothiocarbamoyl chloride (1986-08-9) + p-chlorophenyldithiocarbamic acid triethylamine salt (43009-19-4) → 4-p-chlorophenyl-5-phenylimino-3-thio-1,2,4-thiadiazolidine (40288-26-4) + 4-(4-chloro-phenyl)-5-(4-chloro-phenylimino)-[1,2,4]dithiazolidine-3-thione (23509-92-4)

Guidance literature:

In benzene; Ambient temperature;

Reference yield:

N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride (5180-19-8) + ammonium salt of N-p-chlorophenylamino dithiocarbamic acid (1197-56-4) → 4-(4-chloro-phenyl)-5-(4-chloro-phenylimino)-[1,2,4]dithiazolidine-3-thione (23509-92-4)

Guidance literature:

In benzene;

upstream raw materials:

N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride

ammonium salt of N-p-chlorophenylamino dithiocarbamic acid

p-chlorophenyldithiocarbamic acid triethylamine salt

S-chloro-N-phenylisothiocarbamoyl chloride

Downstream raw materials:

4-p-Chlorphenyl-5-p-chlorphenylimino-1,2,4-dithiazolidin-3-on