3(2H)-Pyridazinone, 5-(4-morpholinylmethyl)-6-phenyl-, hydrazone

Base Information

Chemical Name:3(2H)-Pyridazinone, 5-(4-morpholinylmethyl)-6-phenyl-, hydrazone
CAS No.:99877-37-9
Molecular Formula:C15H19N5O
Molecular Weight:285.3443
Hs Code.:
DSSTox Substance ID:DTXSID20244282
Wikidata:Q83128599

Synonyms:BRN 5095816;99877-37-9;3(2H)-Pyridazinone, 5-(4-morpholinylmethyl)-6-phenyl-, hydrazone;5-(4-Morpholinylmethyl)-6-phenyl-3(2H)-pyridazinone hydrazone;6-Fenil-5-(1-morfolinilmetil)-3-hidrazinopiridazina [Spanish];6-Fenil-5-(1-morfolinilmetil)-3-hidrazinopiridazina;4-((6-Hydrazono-3-phenyl-1,6-dihydropyridazin-4-yl)methyl)morpholine;DTXSID20244282;LS-130056

Suppliers and Price of 3(2H)-Pyridazinone, 5-(4-morpholinylmethyl)-6-phenyl-, hydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3(2H)-Pyridazinone, 5-(4-morpholinylmethyl)-6-phenyl-, hydrazone

Chemical Property:

Vapor Pressure:1.88E-11mmHg at 25°C
Boiling Point:533.3°Cat760mmHg
Flash Point:276.3°C
Density:1.266g/cm³
XLogP3:0.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:285.15896025
Heavy Atom Count:21
Complexity:304

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCN1CC2=CC(=NN=C2C3=CC=CC=C3)NN

Technology Process of 3(2H)-Pyridazinone, 5-(4-morpholinylmethyl)-6-phenyl-, hydrazone

There total 5 articles about 3(2H)-Pyridazinone, 5-(4-morpholinylmethyl)-6-phenyl-, hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 99877-29-9
6-phenyl-5(1-morpholinylmethyl)-3-cloropyridazine

: 99877-37-9
6-phenyl-5-(1-morpholinylmethyl)-3-hydrazinopyridazine

Guidance literature:: With hydrazine hydrate; In ethanol; 1.) 3 h, reflux; 2.) 12 h, 0 deg C;

Reference yield:

: 69797-45-1
6-phenyl-5(1-morpholinylmethyl)-4,5-dihydro-3(2H)-pyridazinone

: 99877-37-9
6-phenyl-5-(1-morpholinylmethyl)-3-hydrazinopyridazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) bromine; 2.) 25 percent NH₄OH / 1.) glacial acetic acid, 2 h, 60-70 deg C

2: 82 percent / POCl₃ / 0 °C

3: 85 percent / 98 percent hydrazine hydrate / ethanol / 1.) 3 h, reflux; 2.) 12 h, 0 deg C

With ammonium hydroxide; bromine; hydrazine hydrate; trichlorophosphate; In ethanol;

Reference yield:

: 69797-31-5
β-(1-morpholinylmethyl)-β-benzoylpropionic acid

: 99877-37-9
6-phenyl-5-(1-morpholinylmethyl)-3-hydrazinopyridazine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / 98 percent hydrazine hydrate / ethanol / 2 h / Heating

2: 1.) bromine; 2.) 25 percent NH₄OH / 1.) glacial acetic acid, 2 h, 60-70 deg C

3: 82 percent / POCl₃ / 0 °C

4: 85 percent / 98 percent hydrazine hydrate / ethanol / 1.) 3 h, reflux; 2.) 12 h, 0 deg C

With ammonium hydroxide; bromine; hydrazine hydrate; trichlorophosphate; In ethanol;