Ccris 6982

Base Information

Chemical Name:Ccris 6982
CAS No.:140461-57-0
Molecular Formula:C21H15NO3
Molecular Weight:329.37
Hs Code.:
Nikkaji Number:J473.519F
Mol file:140461-57-0.mol

Synonyms:CCRIS 6982;(+)-11R,10S-Dihydroxy-9S,8R-epoxy-8,9,10,11-tetrahydrodibenz(a,h)acridine;11S,10R-Dihydroxy-9S,8R-epoxide-8,9,10,11-tetrahydrobenz(a,h)acridine;140461-57-0;Benz(a)oxireno(5,6)benz(1,2-h)acridine-2,3-diol, 1a,2,3,13c-tetrahydro-, (1a-alpha,2-beta,3-alpha,13c-alpha)-(+)-;(1aalpha,2beta,3alpha,13Calpha)-(+)-1a,2,3,13c-tetrahydrobenz(a)oxireno(5,6)benz(1,2-h)acridine-2,3-diol;LS-42576;[8R,(+)]-8beta,9beta-Epoxy-8,9,10,11-tetrahydrodibenz[a,h]acridine-10beta,11alpha-diol;(1AALPHA,2BETA,3ALPHA,13CALPHA)-(+)-1A,2,3,13C-TETRAHYDROBENZ[A]OXIRENO[5,6]BENZ[1,2-H]ACRIDINE-2,3- DIOL

Suppliers and Price of Ccris 6982

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Ccris 6982

Chemical Property:

Vapor Pressure:3.42E-18mmHg at 25°C
Boiling Point:657.7°Cat760mmHg
Flash Point:351.5°C
Density:1.527g/cm³
XLogP3:2.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:329.10519334
Heavy Atom Count:25
Complexity:541

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=C2C=C4C=CC5=C(C4=N3)C6C(O6)C(C5O)O
Isomeric SMILES:C1=CC=C2C(=C1)C=CC3=C2C=C4C=CC5=C(C4=N3)[C@@H]6[C@@H](O6)[C@H]([C@@H]5O)O

Technology Process of Ccris 6982

There total 5 articles about Ccris 6982 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.7%

: 140460-91-9,110927-22-5
(+)-trans-(10R,11R)-dihydroxy-8,9,10,11-tetrahydrodibenzacridine

: 140461-57-0
(+)-(8R,9S,10S,11R)-10,11-dihydroxy-8,9-epoxy-8,9,10,11-tetrahydrodibenzyacridine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; for 2.5h; Ambient temperature;
DOI:10.1021/jo00036a006

Reference yield:

: 97135-18-7,110927-22-5
(+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine

: 140461-57-0
(+)-(8R,9S,10S,11R)-10,11-dihydroxy-8,9-epoxy-8,9,10,11-tetrahydrodibenzyacridine

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / pyridine / 24 h / 0 - 5 °C

2: 89 percent / 10percent aq. NaOH / tetrahydrofuran; methanol / 0.5 h / 0 - 5 °C

3: 84.7 percent / m-CPBA / tetrahydrofuran / 2.5 h / Ambient temperature

With pyridine; sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jo00036a006

Reference yield:

: 97135-19-8,102421-97-6,140460-94-2,140460-95-3
(+/-)-trans-(10,11)-dihydroxy-8,9,10,11-tetrahydrodibenzacridine

: 140461-57-0
(+)-(8R,9S,10S,11R)-10,11-dihydroxy-8,9-epoxy-8,9,10,11-tetrahydrodibenzyacridine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 24 h / Ambient temperature

2: 10percent aq. NaOH / tetrahydrofuran; methanol / 0.5 h / 0 - 5 °C

3: 84.7 percent / m-CPBA / tetrahydrofuran / 2.5 h / Ambient temperature

With pyridine; sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jo00036a006