N-Benzyloxycarbonyl-L-glutamic anhydride

Base Information

Chemical Name:N-Benzyloxycarbonyl-L-glutamic anhydride
CAS No.:84668-91-7
Molecular Formula:C13H13NO5
Molecular Weight:263.24600
Hs Code.:
European Community (EC) Number:223-930-0,622-072-8
DSSTox Substance ID:DTXSID10961517
Mol file:84668-91-7.mol

Synonyms:N-Benzyloxycarbonyl-L-glutamic anhydride;benzyl N-(2,6-dioxooxan-3-yl)carbamate;4124-76-9;[(3R)-Tetrahydro-2,6-dioxo-2H-pyran-3-yl]-carbamic Acid Phenylmethyl;EINECS 223-930-0;SCHEMBL6794132;DTXSID10961517;carbobenzyloxy-l-glutamic anhydride;AKOS024332814;FT-0674994;Benzyl hydrogen (2,6-dioxooxan-3-yl)carbonimidate

Suppliers and Price of N-Benzyloxycarbonyl-L-glutamic anhydride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of N-Benzyloxycarbonyl-L-glutamic anhydride

Chemical Property:

Melting Point:103 - 105 °C
PSA：81.70000
LogP:1.53590
XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:263.07937252
Heavy Atom Count:19
Complexity:362

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC(=O)OC(=O)C1NC(=O)OCC2=CC=CC=C2

Technology Process of N-Benzyloxycarbonyl-L-glutamic anhydride

There total 5 articles about N-Benzyloxycarbonyl-L-glutamic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1155-62-0,5619-01-2,63648-73-7
N-benzyloxycarbonyl-DL-glutamic acid

: 84668-91-7
N-((benzyloxy)carbonyl)glutamic anhydride

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; 1.) 1 h, 0 deg C, 2.) 24 h, r.t.;
DOI:10.1246/bcsj.62.2748

Reference yield:

: 617-65-2,21675-62-7,23009-64-5,25104-13-6,84960-48-5,25513-46-6
Glutamic acid

: 84668-91-7
N-((benzyloxy)carbonyl)glutamic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent

2: 96 percent / dicyclohexylcarbodiimide / ethyl acetate / 1.) 1 h, 0 deg C, 2.) 24 h, r.t.

With dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1246/bcsj.62.2748

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 84668-91-7
N-((benzyloxy)carbonyl)glutamic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent

2: 96 percent / dicyclohexylcarbodiimide / ethyl acetate / 1.) 1 h, 0 deg C, 2.) 24 h, r.t.

With dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1246/bcsj.62.2748