Technology Process of 9-diazofluorene-2-butyric acid
There total 8 articles about 9-diazofluorene-2-butyric acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
2: Wolff-Kishner redn.
3: 45 percent / 70percent sodium bis(2-methoxyethoxy)-aluminum hydride / toluene; benzene
4: 68 percent / 40percent benzyltrimethylammonium hydroxide, O2 / pyridine
5: 67 percent / methanol
6: 77 percent / Jones' reagent / acetone / -10 °C
7: 46 percent / sodium methoxide / methanol / 6 h / 45 °C
With
jones' reagent; oxygen; sodium methylate; N-benzyl-trimethylammonium hydroxide; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
pyridine; methanol; acetone; toluene; benzene;
DOI:10.1039/c39890000636
- Guidance literature:
-
Multi-step reaction with 6 steps
1: Wolff-Kishner redn.
2: 45 percent / 70percent sodium bis(2-methoxyethoxy)-aluminum hydride / toluene; benzene
3: 68 percent / 40percent benzyltrimethylammonium hydroxide, O2 / pyridine
4: 67 percent / methanol
5: 77 percent / Jones' reagent / acetone / -10 °C
6: 46 percent / sodium methoxide / methanol / 6 h / 45 °C
With
jones' reagent; oxygen; sodium methylate; N-benzyl-trimethylammonium hydroxide; sodium bis(2-methoxyethoxy)aluminium dihydride;
In
pyridine; methanol; acetone; toluene; benzene;
DOI:10.1039/c39890000636
