Cyclopropaneacetic acid, 1-(4-bromophenyl)-

Base Information

Chemical Name:Cyclopropaneacetic acid, 1-(4-bromophenyl)-
CAS No.:847359-06-2
Molecular Formula:C11H11BrO2
Molecular Weight:255.111
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopropaneacetic acid, 1-(4-bromophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopropaneacetic acid, 1-(4-bromophenyl)-

There total 3 articles about Cyclopropaneacetic acid, 1-(4-bromophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98480-31-0
(1-(4-bromophenyl)cyclopropyl)methanol

: 847359-06-2
[1-(4-bromophenyl)cyclopropyl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; methanesulfonyl chloride / dichloromethane / -78 - 0 °C

1.2: 3 h / 70 °C

2.1: potassium hydroxide; water / ethanol / Reflux

With water; methanesulfonyl chloride; triethylamine; potassium hydroxide; In ethanol; dichloromethane;

Reference yield:

: 638220-35-6
1-(4-bromophenyl)-cyclopropanecarboxylic acid methyl ester

: 847359-06-2
[1-(4-bromophenyl)cyclopropyl]acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -4 °C

2.1: triethylamine / dichloromethane / 3 h / -78 - 0 °C

3.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

4.1: sodium hydroxide / methanol; water / 16 h / 60 °C

4.2: pH 3

With lithium aluminium tetrahydride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: C₁₁H₁₃BrO₃S

: 847359-06-2
[1-(4-bromophenyl)cyclopropyl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

2.1: sodium hydroxide / methanol; water / 16 h / 60 °C

2.2: pH 3

With triethylamine; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;