1,3-Benzenedicarboxylic acid, 5-[[[2-[3-(1,1-dimethylethoxy)-3-oxopropoxy]-1,1-bis[[3-(1,1-dimethyleth oxy)-3-oxopropoxy]methyl]ethyl]amino]carbonyl]-, bis(pentafluorophenyl) ester

Base Information

Chemical Name:1,3-Benzenedicarboxylic acid, 5-[[[2-[3-(1,1-dimethylethoxy)-3-oxopropoxy]-1,1-bis[[3-(1,1-dimethyleth oxy)-3-oxopropoxy]methyl]ethyl]amino]carbonyl]-, bis(pentafluorophenyl) ester
CAS No.:847375-84-2
Molecular Formula:C46H49F10NO14
Molecular Weight:1029.88
Hs Code.:

1,3-Benzenedicarboxylic acid,
5-[[[2-[3-(1,1-dimethylethoxy)-3-oxopropoxy]-1,1-bis[[3-(1,1-dimethyleth
oxy)-3-oxopropoxy]methyl]ethyl]amino]carbonyl]-, bis(pentafluorophenyl)
ester

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Chemical Property of 1,3-Benzenedicarboxylic acid, 5-[[[2-[3-(1,1-dimethylethoxy)-3-oxopropoxy]-1,1-bis[[3-(1,1-dimethyleth oxy)-3-oxopropoxy]methyl]ethyl]amino]carbonyl]-, bis(pentafluorophenyl) ester

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Technology Process of 1,3-Benzenedicarboxylic acid, 5-[[[2-[3-(1,1-dimethylethoxy)-3-oxopropoxy]-1,1-bis[[3-(1,1-dimethyleth oxy)-3-oxopropoxy]methyl]ethyl]amino]carbonyl]-, bis(pentafluorophenyl) ester

There total 4 articles about 1,3-Benzenedicarboxylic acid, 5-[[[2-[3-(1,1-dimethylethoxy)-3-oxopropoxy]-1,1-bis[[3-(1,1-dimethyleth oxy)-3-oxopropoxy]methyl]ethyl]amino]carbonyl]-, bis(pentafluorophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1-(tris{[2-(tert-butoxycarbonyl)ethoxy]methyl}methylaminocarbonyl)benzene-3,5-dicarboxylic acid

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 847375-84-2
1-(tris{[2-(tert-butoxycarbonyl)ethoxy]methyl}methylaminocarbonyl)benzene-3,5-dicarboxylic acid bis(pentafluorophenyl) ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 - 20 ℃; for 4h;
DOI:10.1002/anie.200461409

Reference yield:

: 4422-95-1
1,3,5-benzene tris(carbonyl chloride)

: 847375-84-2
1-(tris{[2-(tert-butoxycarbonyl)ethoxy]methyl}methylaminocarbonyl)benzene-3,5-dicarboxylic acid bis(pentafluorophenyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-diisopropylethylamine / tetrahydrofuran / 17 h / 20 °C

1.2: 67 percent / sodium hydroxide / H₂O; tetrahydrofuran

2.1: 87 percent / N,N'-dicyclohexylcarbodiimide / tetrahydrofuran / 4 h / 0 - 20 °C

With N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1002/anie.200461409

Reference yield:

: 175724-30-8
tris{[2-(tert-butoxycarbonyl)ethoxy]methyl}methylamine

: 847375-84-2
1-(tris{[2-(tert-butoxycarbonyl)ethoxy]methyl}methylaminocarbonyl)benzene-3,5-dicarboxylic acid bis(pentafluorophenyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-diisopropylethylamine / tetrahydrofuran / 17 h / 20 °C

1.2: 67 percent / sodium hydroxide / H₂O; tetrahydrofuran

2.1: 87 percent / N,N'-dicyclohexylcarbodiimide / tetrahydrofuran / 4 h / 0 - 20 °C

With N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1002/anie.200461409