Carbamic acid, [2-[[[4-(2-furanyl)-6-[(octahydro-1H-1,4,7-triazonin-1-yl)methyl]-2-pyridin yl]carbonyl]amino]ethyl]-, (4-nitrophenyl)methyl ester

Base Information

• Chemical Name: Carbamic acid, [2-[[[4-(2-furanyl)-6-[(octahydro-1H-1,4,7-triazonin-1-yl)methyl]-2-pyridin yl]carbonyl]amino]ethyl]-, (4-nitrophenyl)methyl ester
• CAS No.: 847454-21-1
• Molecular Formula: C27H33N7O6
• Molecular Weight: 551.602

Synonyms:

Chemical Property of Carbamic acid, [2-[[[4-(2-furanyl)-6-[(octahydro-1H-1,4,7-triazonin-1-yl)methyl]-2-pyridin yl]carbonyl]amino]ethyl]-, (4-nitrophenyl)methyl ester

Chemical Property:

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Technology Process of Carbamic acid, [2-[[[4-(2-furanyl)-6-[(octahydro-1H-1,4,7-triazonin-1-yl)methyl]-2-pyridin yl]carbonyl]amino]ethyl]-, (4-nitrophenyl)methyl ester

There total 1 articles about Carbamic acid, [2-[[[4-(2-furanyl)-6-[(octahydro-1H-1,4,7-triazonin-1-yl)methyl]-2-pyridin yl]carbonyl]amino]ethyl]-, (4-nitrophenyl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-(4-(furan-2-yl)-6-[2-(4-nitrobenzyloxycarbonylamino)ethylcarbamoyl]pyridin-2-ylmethyl)-1,4,7-triazacyclononane-1,4-dicarboxylic acid di-tert-butyl ester (847454-20-0) → (2-([4-(furan-2-yl)-6-(1,4,7-triazacyclononanyl-1-methyl)pyridine-2-carbonyl]amino)ethyl)carbamic acid 4-nitrobenzyl ester (847454-21-1)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 0.5h;

Reference yield:

6-(bromomethyl)-4-(furan-2-yl) pyridine-2-carboxylic acid ethyl ester (847454-17-5) + (2-([4-(furan-2-yl)-6-(1,4,7-triazacyclononanyl-1-methyl)pyridine-2-carbonyl]amino)ethyl)carbamic acid 4-nitrobenzyl ester (847454-21-1) → (2-((4-(furan-2-yl)-6-(4,7-bis[6-ethoxycarbonyl-4-(furan-2-yl)pyridin-2-ylmethyl]-1,4,7-triazacyclononanyl-1-methyl)pyridine-2-carbonyl)amino)ethyl)carbamic acid 4-nitrobenzyl ester (847454-22-2)

Guidance literature:

With potassium carbonate; In acetonitrile; for 3h; Heating / reflux;

upstream raw materials:

7-(4-(furan-2-yl)-6-[2-(4-nitrobenzyloxycarbonylamino)ethylcarbamoyl]pyridin-2-ylmethyl)-1,4,7-triazacyclononane-1,4-dicarboxylic acid di-tert-butyl ester

Downstream raw materials:

(2-((4-(furan-2-yl)-6-(4,7-bis[6-ethoxycarbonyl-4-(furan-2-yl)pyridin-2-ylmethyl]-1,4,7-triazacyclononanyl-1-methyl)pyridine-2-carbonyl)amino)ethyl)carbamic acid 4-nitrobenzyl ester

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