Bis[(4-methylphenyl)sulfanyl]acetic acid

Base Information

Chemical Name:Bis[(4-methylphenyl)sulfanyl]acetic acid
CAS No.:17067-32-2
Molecular Formula:C16H16O2S2
Molecular Weight:304.427
Hs Code.:
NSC Number:122665
DSSTox Substance ID:DTXSID70298356
Wikidata:Q82040122
Mol file:17067-32-2.mol

Synonyms:17067-32-2;bis[(4-methylphenyl)sulfanyl]acetic acid;NSC122665;DTXSID70298356;NSC-122665

Suppliers and Price of Bis[(4-methylphenyl)sulfanyl]acetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of Bis[(4-methylphenyl)sulfanyl]acetic acid

Chemical Property:

Vapor Pressure:6.07E-09mmHg at 25°C
Boiling Point:451.6°Cat760mmHg
Flash Point:226.9°C
Density:1.27g/cm³
XLogP3:5.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:304.05917210
Heavy Atom Count:20
Complexity:282

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)SC(C(=O)O)SC2=CC=C(C=C2)C

Technology Process of Bis[(4-methylphenyl)sulfanyl]acetic acid

There total 6 articles about Bis[(4-methylphenyl)sulfanyl]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: Chloro-p-tolylsulfanyl-acetic acid ethyl ester

: 17067-32-2
2,2-bis(p-tolylthio)acetic acid

: ethyl 2,2-bis(p-tolylthio)acetate

Guidance literature:: With aluminum oxide; at 120 ℃; for 24h;

Reference yield:

: 3996-42-7
2-[(4-methylphenyl)sulfinyl] acetic acid

: 17067-32-2
2,2-bis(p-tolylthio)acetic acid

Guidance literature:: With dihydrogen peroxide; In acetic acid;
DOI:10.1021/ja01480a016

Reference yield:

: 14738-27-3
ethyl (p-tolylthio)acetate

: 17067-32-2
2,2-bis(p-tolylthio)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl chloride / CH₂Cl₂ / Heating

2: 12 percent / alumina / 24 h / 120 °C

With aluminum oxide; sulfuryl dichloride; In dichloromethane;