9-(4-Aminophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione

Base Information

Chemical Name:9-(4-Aminophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione
CAS No.:847658-75-7
Molecular Formula:C23H28N2O2
Molecular Weight:364.488
Hs Code.:
DSSTox Substance ID:DTXSID701127048

Synonyms:DTXSID701127048;9-(4-Aminophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione;847658-75-7

Suppliers and Price of 9-(4-Aminophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(4-Aminophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:364.215078140
Heavy Atom Count:27
Complexity:696

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(CC2=C(C(C3=C(N2)CC(CC3=O)(C)C)C4=CC=C(C=C4)N)C(=O)C1)C

Technology Process of 9-(4-Aminophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione

There total 6 articles about 9-(4-Aminophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 3357-14-0
3,3,6,6-tetramethyl-9-(4-nitrophenyl)-1,8-dioxodecahydroacridine

: 847658-75-7
9-(4-aminophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

Guidance literature:: With calcium chloride; zinc; In ethanol; water; for 2h; Heating;
DOI:10.1021/ol047463k

Reference yield:

: 556-18-3,28107-09-7
4-aminobenzaldehyde

: 126-81-8
dimedone

: 847658-75-7
9-(4-aminophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

Guidance literature:: With ferrite; ammonium acetate; In neat (no solvent); at 120 ℃;
DOI:10.13005/ojc/310347

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 847658-75-7
9-(4-aminophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H)-acridinedione

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; H₂O / Heating

2: ammonium acetate; acetic acid / 6 h / Heating

3: 70 percent / zinc; CaCl₂ / ethanol; H₂O / 2 h / Heating

With ammonium acetate; acetic acid; calcium chloride; zinc; In methanol; ethanol; water;
DOI:10.1021/ol047463k