3-(trifluoromethyl)-N-[3-(trifluoromethyl)phenyl]benzamide

Base Information

Chemical Name:3-(trifluoromethyl)-N-[3-(trifluoromethyl)phenyl]benzamide
CAS No.:34556-78-0
Molecular Formula:C15H9F6NO
Molecular Weight:333.233
Hs Code.:

Synonyms:3-(trifluoromethyl)-N-[3-(trifluoromethyl)phenyl]benzamide;3-Trifluoromethyl-N-(3-trifluoromethyl-phenyl)-benzamide;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(trifluoromethyl)-N-[3-(trifluoromethyl)phenyl]benzamide

Chemical Property:

Vapor Pressure:0.00441mmHg at 25°C
Melting Point:126 - 128 °C
Boiling Point:277.9°Cat760mmHg
Flash Point:121.8°C
PSA：29.10000
Density:1.416g/cm³
LogP:5.04950

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3-(trifluoromethyl)-N-[3-(trifluoromethyl)phenyl]benzamide

There total 4 articles about 3-(trifluoromethyl)-N-[3-(trifluoromethyl)phenyl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 98-16-8
3-trifluoromethylaniline

: 2251-65-2
3-(Trifluoromethyl)benzoyl chloride

: 34556-78-0
3-(trifluoromethyl)-N-[3-(trifluoromethyl)phenyl]benzamide

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1039/c2ce06254b

Reference yield:

: 2646-97-1
3-(trifluoromethyl)-aniline hydrochloride

: 2251-65-2
3-(Trifluoromethyl)benzoyl chloride

: 34556-78-0
3-(trifluoromethyl)-N-[3-(trifluoromethyl)phenyl]benzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1002/anie.201307377

Reference yield:

: 454-92-2
3-(trifluoromethyl)benzoic acid

: 34556-78-0
3-(trifluoromethyl)-N-[3-(trifluoromethyl)phenyl]benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 0 °C

2: triethylamine / dichloromethane / 0 °C

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/anie.201307377